C₂₅H₃₈O₇SSi

Base Information

Chemical Name:C₂₅H₃₈O₇SSi
CAS No.:902120-07-4
Molecular Formula:C₂₅H₃₈O₇SSi
Molecular Weight:510.724
Hs Code.:

C<sub>25</sub>H<sub>38</sub>O<sub>7</sub>SSi

Synonyms:C₂₅H₃₈O₇SSi

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Chemical Property of C₂₅H₃₈O₇SSi

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Technology Process of C₂₅H₃₈O₇SSi

There total 15 articles about C₂₅H₃₈O₇SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-71-1
3-Hydroxyacetophenone

: 902120-07-4
C₂₅H₃₈O₇SSi

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / MeONa / methanol / 96 h / 20 °C

2: 85 percent / H₂ / PtO₂ / ethyl acetate; CH₂Cl₂ / 4 h / 760.05 Torr

3: 94 percent / (S)-tetrahydro-1-Bu-3,3-Ph₂-pyrrolo[1,2-c][1,3,2]oxazaborole; BH₃*Me₂S / toluene; tetrahydrofuran / 0.33 h / 20 °C

4: 63 percent / imidazole / CH₂Cl₂ / 12 h / 20 °C

5: Et₃N / CH₂Cl₂ / 0.5 h / cooling

With 1H-imidazole; dimethylsulfide borane complex; hydrogen; sodium methylate; triethylamine; platinum(IV) oxide; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; toluene; 3: Corey-Bakshi-Shibata reduction;
DOI:10.1039/b603857c

Reference yield:

: 178445-81-3
(E)-1-(3-hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)prop-2-en-1-one

: 902120-07-4
C₂₅H₃₈O₇SSi

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / H₂ / PtO₂ / ethyl acetate; CH₂Cl₂ / 4 h / 760.05 Torr

2: 94 percent / (S)-tetrahydro-1-Bu-3,3-Ph₂-pyrrolo[1,2-c][1,3,2]oxazaborole; BH₃*Me₂S / toluene; tetrahydrofuran / 0.33 h / 20 °C

3: 63 percent / imidazole / CH₂Cl₂ / 12 h / 20 °C

4: Et₃N / CH₂Cl₂ / 0.5 h / cooling

With 1H-imidazole; dimethylsulfide borane complex; hydrogen; triethylamine; platinum(IV) oxide; In tetrahydrofuran; dichloromethane; ethyl acetate; toluene; 2: Corey-Bakshi-Shibata reduction;
DOI:10.1039/b603857c

Reference yield:

: 178445-84-6
1-(3-hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)-1-propanone

: 902120-07-4
C₂₅H₃₈O₇SSi

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / (S)-tetrahydro-1-Bu-3,3-Ph₂-pyrrolo[1,2-c][1,3,2]oxazaborole; BH₃*Me₂S / toluene; tetrahydrofuran / 0.33 h / 20 °C

2: 63 percent / imidazole / CH₂Cl₂ / 12 h / 20 °C

3: Et₃N / CH₂Cl₂ / 0.5 h / cooling

With 1H-imidazole; dimethylsulfide borane complex; triethylamine; In tetrahydrofuran; dichloromethane; toluene; 1: Corey-Bakshi-Shibata reduction;
DOI:10.1039/b603857c