3,3'-(5-tert-butyl-2-hydroxy-1,3-phenylene)bis(methylene)bis(1-(5-tert-butyl-2-hydroxybenzyl)imidazolidine-2-thione)

Base Information

• Chemical Name: 3,3'-(5-tert-butyl-2-hydroxy-1,3-phenylene)bis(methylene)bis(1-(5-tert-butyl-2-hydroxybenzyl)imidazolidine-2-thione)
• CAS No.: 1266201-01-7
• Molecular Formula: C₄₀H₅₄N₄O₃S₂
• Molecular Weight: 703.026

Synonyms:3,3'-(5-tert-butyl-2-hydroxy-1,3-phenylene)bis(methylene)bis(1-(5-tert-butyl-2-hydroxybenzyl)imidazolidine-2-thione)

Chemical Property of 3,3'-(5-tert-butyl-2-hydroxy-1,3-phenylene)bis(methylene)bis(1-(5-tert-butyl-2-hydroxybenzyl)imidazolidine-2-thione)

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Technology Process of 3,3'-(5-tert-butyl-2-hydroxy-1,3-phenylene)bis(methylene)bis(1-(5-tert-butyl-2-hydroxybenzyl)imidazolidine-2-thione)

There total 3 articles about 3,3'-(5-tert-butyl-2-hydroxy-1,3-phenylene)bis(methylene)bis(1-(5-tert-butyl-2-hydroxybenzyl)imidazolidine-2-thione) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

N,N'-ethylenethiourea (96-45-7) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + para-tert-butylphenol (98-54-4) → linear S-tert-butylphenol-calix[1,1]urene (1266200-98-9) + 1,3-bis(5-tert-butyl-2-hydroxybenzyl)imidazolidine-2-thione (1266201-29-9) + 3,3'-(5-tert-butyl-2-hydroxy-1,3-phenylene)bis(methylene)bis(1-(5-tert-butyl-2-hydroxybenzyl)imidazolidine-2-thione) (1266201-01-7)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 70 ℃; for 96h;

Reference yield: 24.0%

N,N'-ethylenethiourea (96-45-7) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + para-tert-butylphenol (98-54-4) → 3,3'-(5-tert-butyl-2-hydroxy-1,3-phenylene)bis(methylene)bis(1-(5-tert-butyl-2-hydroxybenzyl)imidazolidine-2-thione) (1266201-01-7) + 3,3'-(3,3'-(2-thioxoimidazolidine-1,3-diyl)bis(methylene)bis(5-tert-butyl-2-hydroxy-3,1-phenylene)bis(methylene))bis(1-(5-tert-butyl-2-hydroxybenzyl)imidazolidine-2-thione) (1266201-04-0)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 70 ℃; for 96h;

DOI:10.1039/c3cc48284g

Reference yield: 9.9%

N,N'-ethylenethiourea (96-45-7) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + para-tert-butylphenol (98-54-4) → linear S-tert-butylphenol-calix[1,1]urene (1266200-98-9) + 1,3-bis(5-tert-butyl-2-hydroxybenzyl)imidazolidine-2-thione (1266201-29-9) + 3,3'-(5-tert-butyl-2-hydroxy-1,3-phenylene)bis(methylene)bis(1-(5-tert-butyl-2-hydroxybenzyl)imidazolidine-2-thione) (1266201-01-7) + 3,3'-(3,3'-(2-thioxoimidazolidine-1,3-diyl)bis(methylene)bis(5-tert-butyl-2-hydroxy-3,1-phenylene)bis(methylene))bis(1-(5-tert-butyl-2-hydroxybenzyl)imidazolidine-2-thione) (1266201-04-0)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 70 ℃; for 96h;

upstream raw materials:

N,N'-ethylenethiourea

formaldehyd

para-tert-butylphenol

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