4-(benzyloxy)-5-carbamoyl-3-β-ribofuranosylpyrazolyl(5->5')adenosine pyrophosphate

Base Information

Chemical Name:4-(benzyloxy)-5-carbamoyl-3-β-ribofuranosylpyrazolyl(5->5')adenosine pyrophosphate
CAS No.:99298-33-6
Molecular Formula:C₂₆H₃₂N₈O₁₅P₂
Molecular Weight:758.532
Hs Code.:

Synonyms:4-(benzyloxy)-5-carbamoyl-3-β-ribofuranosylpyrazolyl(5->5')adenosine pyrophosphate

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Chemical Property of 4-(benzyloxy)-5-carbamoyl-3-β-ribofuranosylpyrazolyl(5->5')adenosine pyrophosphate

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Technology Process of 4-(benzyloxy)-5-carbamoyl-3-β-ribofuranosylpyrazolyl(5->5')adenosine pyrophosphate

There total 4 articles about 4-(benzyloxy)-5-carbamoyl-3-β-ribofuranosylpyrazolyl(5->5')adenosine pyrophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.6%

: 694428-93-8
4-(benzyloxy)-3-β-D-ribofuranosylpyrazole-5-carboxamide 5'-monophosphate

: 57816-25-8
adenosine 5'-phosphoric di-n-butylphosphinothioic anhydride

: 99298-33-6
4-(benzyloxy)-5-carbamoyl-3-β-ribofuranosylpyrazolyl(5->5')adenosine pyrophosphate

Guidance literature:: With pyridine; silver nitrate;
DOI:10.1021/jm00152a016

Reference yield:

: 100-39-0
benzyl bromide

: 99298-33-6
4-(benzyloxy)-5-carbamoyl-3-β-ribofuranosylpyrazolyl(5->5')adenosine pyrophosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 87.4 percent / Na₂CO₃ / H₂O; acetonitrile / 18 h / Ambient temperature

2: POCl₃, trimethylphosphate / 2 h / 0 - 5 °C

3: 90.6 percent / AgNO₃, pyridine

With pyridine; trimethyl phosphite; sodium carbonate; silver nitrate; trichlorophosphate; In water; acetonitrile;
DOI:10.1021/jm00152a016

Reference yield:

: 30868-30-5
pyrazofurin

: 99298-33-6
4-(benzyloxy)-5-carbamoyl-3-β-ribofuranosylpyrazolyl(5->5')adenosine pyrophosphate

Guidance literature:: Multi-step reaction with 3 steps

1: 87.4 percent / Na₂CO₃ / H₂O; acetonitrile / 18 h / Ambient temperature

2: POCl₃, trimethylphosphate / 2 h / 0 - 5 °C

3: 90.6 percent / AgNO₃, pyridine

With pyridine; trimethyl phosphite; sodium carbonate; silver nitrate; trichlorophosphate; In water; acetonitrile;
DOI:10.1021/jm00152a016