[ZrCl₂(C₅H₄CH₂NH₂C₆H₃(CH(CH₃)2)2)(C₅H₄CH₂NHC₆H₃(CH(CH₃)2)2)]⁽¹⁺⁾*[HB(C₆F₅)3]^(1-)=C₅₄H₅₀BCl₂F₁₅N₂Zr

Base Information

• Chemical Name: [ZrCl₂(C₅H₄CH₂NH₂C₆H₃(CH(CH₃)2)2)(C₅H₄CH₂NHC₆H₃(CH(CH₃)2)2)]⁽¹⁺⁾*[HB(C₆F₅)3]^(1-)=C₅₄H₅₀BCl₂F₁₅N₂Zr
• CAS No.: 1132983-49-3
• Molecular Formula: C₁₈HBF₁₅*C₃₆H₄₉Cl₂N₂Zr
• Molecular Weight: 1184.92

Synonyms:[ZrCl₂(C₅H₄CH₂NH₂C₆H₃(CH(CH₃)2)2)(C₅H₄CH₂NHC₆H₃(CH(CH₃)2)2)]⁽¹⁺⁾*[HB(C₆F₅)3]^(1-)=C₅₄H₅₀BCl₂F₁₅N₂Zr

Chemical Property of [ZrCl₂(C₅H₄CH₂NH₂C₆H₃(CH(CH₃)2)2)(C₅H₄CH₂NHC₆H₃(CH(CH₃)2)2)]⁽¹⁺⁾*[HB(C₆F₅)3]^(1-)=C₅₄H₅₀BCl₂F₁₅N₂Zr

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Technology Process of [ZrCl₂(C₅H₄CH₂NH₂C₆H₃(CH(CH₃)2)2)(C₅H₄CH₂NHC₆H₃(CH(CH₃)2)2)]⁽¹⁺⁾*[HB(C₆F₅)3]^(1-)=C₅₄H₅₀BCl₂F₁₅N₂Zr

There total 3 articles about [ZrCl₂(C₅H₄CH₂NH₂C₆H₃(CH(CH₃)2)2)(C₅H₄CH₂NHC₆H₃(CH(CH₃)2)2)]⁽¹⁺⁾*[HB(C₆F₅)3]^(1-)=C₅₄H₅₀BCl₂F₁₅N₂Zr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

bis(C5H4CHN-2,6-diisopropylphenyl)zirconium dichloride (1132983-43-7) + tris(pentafluorophenyl)borate (1109-15-5) + hydrogen (1333-74-0) → [ZrCl2(C5H4CH2NH2C6H3(CH(CH3)2)2)2](2+)*2[HB(C6F5)3](1-)=[ZrCl2(C5H4CH2NH2C6H3(CH(CH3)2)2)2][HB(C6F5)3]2 + [ZrCl2(C5H4CH2NH2C6H3(CH(CH3)2)2)(C5H4CH2NHC6H3(CH(CH3)2)2)](1+)*[HB(C6F5)3](1-)=C54H50BCl2F15N2Zr (1132983-49-3)

Guidance literature:

In benzene; under 2 bar H2 overnight; obtained impure;

Reference yield:

bis(C5H4CHN-2,6-diisopropylphenyl)zirconium dichloride (1132983-43-7) + tris(pentafluorophenyl)borate (1109-15-5) + hydrogen (1333-74-0) → bis(C5H4CH2NH-2,6-diisopropylphenyl)zirconium dichloride (1132983-46-0) + [ZrCl2(C5H4CH2NH2C6H3(CH(CH3)2)2)(C5H4CH2NHC6H3(CH(CH3)2)2)](1+)*[HB(C6F5)3](1-)=C54H50BCl2F15N2Zr (1132983-49-3)

Guidance literature:

In benzene; under 2 bar H2 at room temp. overnight; crystd. from pentane at -33°C;

Reference yield:

bis(C5H4CHN-2,6-diisopropylphenyl)zirconium dichloride (1132983-43-7) + tris(pentafluorophenyl)borate (1109-15-5) + hydrogen (1333-74-0) → bis(C5H4CH2NH-2,6-diisopropylphenyl)zirconium dichloride (1132983-46-0) + [ZrCl2(C5H4CH2NH2C6H3(CH(CH3)2)2)2](2+)*2[HB(C6F5)3](1-)=[ZrCl2(C5H4CH2NH2C6H3(CH(CH3)2)2)2][HB(C6F5)3]2 + [ZrCl2(C5H4CH2NH2C6H3(CH(CH3)2)2)(C5H4CH2NHC6H3(CH(CH3)2)2)](1+)*[HB(C6F5)3](1-)=C54H50BCl2F15N2Zr (1132983-49-3)

Guidance literature:

In benzene; under 2 bar H2 at room temp.; not isolated, detected by NMR;

upstream raw materials:

bis(C₅H₄CHN-2,6-diisopropylphenyl)zirconium dichloride

tris(pentafluorophenyl)borate

hydrogen

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