1-(2-tert-Butyloxycarbonyl)hydrazino-1-deoxy-2,3,5-tri-O-benzyl-L-xylitol

Base Information

Chemical Name:1-(2-tert-Butyloxycarbonyl)hydrazino-1-deoxy-2,3,5-tri-O-benzyl-L-xylitol
CAS No.:261761-95-9
Molecular Formula:C₃₁H₄₀N₂O₆
Molecular Weight:536.668
Hs Code.:

Synonyms:1-(2-tert-Butyloxycarbonyl)hydrazino-1-deoxy-2,3,5-tri-O-benzyl-L-xylitol

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Chemical Property of 1-(2-tert-Butyloxycarbonyl)hydrazino-1-deoxy-2,3,5-tri-O-benzyl-L-xylitol

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Technology Process of 1-(2-tert-Butyloxycarbonyl)hydrazino-1-deoxy-2,3,5-tri-O-benzyl-L-xylitol

There total 3 articles about 1-(2-tert-Butyloxycarbonyl)hydrazino-1-deoxy-2,3,5-tri-O-benzyl-L-xylitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 870-46-2
t-butoxycarbonylhydrazine

: 16838-89-4,17073-88-0,60933-68-8,60933-69-9,73068-66-3,89361-52-4,89615-42-9,89615-45-2,96192-07-3
2,3,5-tri-O-benzyl-L-xylofuranose

: 261761-95-9
1-(2-tert-Butyloxycarbonyl)hydrazino-1-deoxy-2,3,5-tri-O-benzyl-L-xylitol

Guidance literature:: With sodium cyanoborohydride; acetic acid; In methanol; at 60 ℃; Inert atmosphere;
DOI:10.1055/s-0039-1690019

Reference yield:

: 41546-31-0
L-xylose

: 261761-95-9
1-(2-tert-Butyloxycarbonyl)hydrazino-1-deoxy-2,3,5-tri-O-benzyl-L-xylitol

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetyl chloride; methanol / 5.5 h / 20 °C / Inert atmosphere

1.2: 0.17 h / 20 °C / Inert atmosphere

2.1: sodium cyanoborohydride; acetic acid / methanol / 60 °C / Inert atmosphere

With methanol; sodium cyanoborohydride; acetic acid; acetyl chloride; In methanol;
DOI:10.1055/s-0039-1690019

Reference yield:

: 100-39-0
benzyl bromide

: 261761-95-9
1-(2-tert-Butyloxycarbonyl)hydrazino-1-deoxy-2,3,5-tri-O-benzyl-L-xylitol

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetyl chloride; methanol / 5.5 h / 20 °C / Inert atmosphere

1.2: 0.17 h / 20 °C / Inert atmosphere

2.1: sodium cyanoborohydride; acetic acid / methanol / 60 °C / Inert atmosphere

With methanol; sodium cyanoborohydride; acetic acid; acetyl chloride; In methanol;
DOI:10.1055/s-0039-1690019