3,5-dimethoxybenzylic diethyl phosphate

Base Information

• Chemical Name: 3,5-dimethoxybenzylic diethyl phosphate
• CAS No.: 292038-60-9
• Molecular Formula: C₁₃H₂₁O₆P
• Molecular Weight: 304.28
• Mol file: 292038-60-9.mol

Synonyms:3,5-dimethoxybenzylic diethyl phosphate

Chemical Property of 3,5-dimethoxybenzylic diethyl phosphate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,5-dimethoxybenzylic diethyl phosphate

There total 1 articles about 3,5-dimethoxybenzylic diethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

3,5-dimethoxybenzyl alcohol (705-76-0) + diethyl chlorophosphate (814-49-3) → 3,5-dimethoxybenzylic diethyl phosphate (292038-60-9)

Guidance literature:

In pyridine; at 0 ℃; for 6h;

DOI:10.1021/jo000387o

Reference yield: 98.7%

4-[N,N-di(p-tolyl)amino]benzaldehyde (42906-19-4) + 3,5-dimethoxybenzylic diethyl phosphate (292038-60-9) → 4'-bis(4-methylphenyl)amino-3,5-dimethoxy-stilbene

Guidance literature:

In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; cyclohexane; N,N-dimethyl-formamide; toluene;

Reference yield:

methanol (67-56-1) + 3,5-dimethoxybenzylic diethyl phosphate (292038-60-9) → 3,5,3',5'-tetramethoxy-bibenzyl (22976-41-6) + 1,3-dimethoxy-5-methylbenzene (4179-19-5) + 1-methylmethoxy-3,5-dimethoxybenzene (73569-69-4)

Guidance literature:

at 25 ℃; Product distribution; Photolysis;

DOI:10.1021/jo000387o

upstream raw materials:

3,5-dimethoxybenzyl alcohol

diethyl chlorophosphate

Downstream raw materials:

3,5,3',5'-tetramethoxy-bibenzyl

1,3-dimethoxy-5-methylbenzene

1-methylmethoxy-3,5-dimethoxybenzene