{SP-4-4-1(R),4(S)}-{1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{2-(methylphenylphosphino)ethanethiolato-P,S}palladium(II)

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Chemical Name:{SP-4-4-1(R),4(S)}-{1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{2-(methylphenylphosphino)ethanethiolato-P,S}palladium(II)
CAS No.:139461-42-0
Molecular Formula:C₂₃H₂₈NPPdS
Molecular Weight:487.942
Hs Code.:

Synonyms:{SP-4-4-1(R),4(S)}-{1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{2-(methylphenylphosphino)ethanethiolato-P,S}palladium(II)

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Chemical Property of {SP-4-4-1(R),4(S)}-{1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{2-(methylphenylphosphino)ethanethiolato-P,S}palladium(II)

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Technology Process of {SP-4-4-1(R),4(S)}-{1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{2-(methylphenylphosphino)ethanethiolato-P,S}palladium(II)

There total 1 articles about {SP-4-4-1(R),4(S)}-{1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{2-(methylphenylphosphino)ethanethiolato-P,S}palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 139493-23-5
chlorobis{(R)-1{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{μ-{(S)-2-(methylphenylphosphino)ethanethiolato-P,S}dipalladium(II)}-dichloromethane

: 139461-42-0
{SP-4-4-1(R),4(S)}-{1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{2-(methylphenylphosphino)ethanethiolato-P,S}palladium(II)

: 102808-70-8
C₁₀H₆CH(CH₃)N(CH₃)2Pd(NH₂CH₂)2⁽¹⁺⁾*Cl^(1-) = C₁₀H₆CH(CH₃)N(CH₃)2Pd(NH₂CH₂)2Cl

Guidance literature:: With diamino-1,2-ethane; In dichloromethane; water; Pd-compound in CH2Cl2 treated with H2NCH2CH2NH2 in H2O, stirred for 1 h (Ar); org. from aq. phases sepd., content of org. phase recrystd. (dichloromethane-methanol mixt.); elem. anal.; aq. phase concd.;

Reference yield: 91.0%

: 139461-42-0
{SP-4-4-1(R),4(S)}-{1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{2-(methylphenylphosphino)ethanethiolato-P,S}palladium(II)

: 100-39-0
benzyl bromide

: 139461-43-1
{SP-4-4-1(R),4(S)}-bromo{1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{1-(benzylthio)-2-(methylphosphino)ethane-P}palladium(II)

Guidance literature:: In dichloromethane; standed for 12 h (Ar); solvent removed, residue recrystd. (acetone-dichloromethane-diethyl ether mixt.); elem. anal.;