chlorobis{(R)-1{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{μ-{(S)-2-(methylphenylphosphino)ethanethiolato-P,S}dipalladium(II)}-dichloromethane

Base Information

Chemical Name:chlorobis{(R)-1{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{μ-{(S)-2-(methylphenylphosphino)ethanethiolato-P,S}dipalladium(II)}-dichloromethane
CAS No.:139493-23-5
Molecular Formula:CH₂Cl₂*C₃₇H₄₄ClN₂PPd₂S
Molecular Weight:913.035
Hs Code.:

chlorobis{(R)-1{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{μ-{(S)-2-(methylphenylphosphino)ethanethiolato-P,S}dipalladium(II)}-dichloromethane

Synonyms:chlorobis{(R)-1{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{μ-{(S)-2-(methylphenylphosphino)ethanethiolato-P,S}dipalladium(II)}-dichloromethane

Suppliers and Price of chlorobis{(R)-1{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{μ-{(S)-2-(methylphenylphosphino)ethanethiolato-P,S}dipalladium(II)}-dichloromethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of chlorobis{(R)-1{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{μ-{(S)-2-(methylphenylphosphino)ethanethiolato-P,S}dipalladium(II)}-dichloromethane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of chlorobis{(R)-1{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{μ-{(S)-2-(methylphenylphosphino)ethanethiolato-P,S}dipalladium(II)}-dichloromethane

There total 1 articles about chlorobis{(R)-1{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{μ-{(S)-2-(methylphenylphosphino)ethanethiolato-P,S}dipalladium(II)}-dichloromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 80145-77-3
(+)589-bis(μ-chloro)bis{(R)-{1-(dimethylamino)ethyl}naphthalenyl-C2,N}dipalladium(II) - 0.5-dichloromethane

: 102782-08-1
(2-mercaptoethyl)methylphenylphosphine

: 139493-23-5
chlorobis{(R)-1{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{μ-{(S)-2-(methylphenylphosphino)ethanethiolato-P,S}dipalladium(II)}-dichloromethane

Guidance literature:: With triethylamine; In dichloromethane; byproducts: {(C2H5)3NH}Cl, (R,R)-(C10H6CH(CH3)N(CH3)2Pd)2ClS(CH2)2P(CH3)C6H5; stirred for 1 h (Ar); washed (water), org. layer sepd., dried (MgSO4), evapd., taked up (dichloromethane), dild. (acetone), concd.; elem. anal.;

Reference yield: 87.0%

: 139493-23-5
chlorobis{(R)-1{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{μ-{(S)-2-(methylphenylphosphino)ethanethiolato-P,S}dipalladium(II)}-dichloromethane

: 139461-42-0
{SP-4-4-1(R),4(S)}-{1-{1-(dimethylamino)ethyl}-2-naphthalenyl-C,N}{2-(methylphenylphosphino)ethanethiolato-P,S}palladium(II)

: 102808-70-8
C₁₀H₆CH(CH₃)N(CH₃)2Pd(NH₂CH₂)2⁽¹⁺⁾*Cl^(1-) = C₁₀H₆CH(CH₃)N(CH₃)2Pd(NH₂CH₂)2Cl

Guidance literature:: With diamino-1,2-ethane; In dichloromethane; water; Pd-compound in CH2Cl2 treated with H2NCH2CH2NH2 in H2O, stirred for 1 h (Ar); org. from aq. phases sepd., content of org. phase recrystd. (dichloromethane-methanol mixt.); elem. anal.; aq. phase concd.;