4-(cyclohexyloxy)-7-methyl-6-[1-(4-methylphenylimino)ethyl]pterin

Base Information

• Chemical Name: 4-(cyclohexyloxy)-7-methyl-6-[1-(4-methylphenylimino)ethyl]pterin
• CAS No.: 1254938-81-2
• Molecular Formula: C₂₂H₂₆N₆O
• Molecular Weight: 390.488
• Mol file: 1254938-81-2.mol

Synonyms:4-(cyclohexyloxy)-7-methyl-6-[1-(4-methylphenylimino)ethyl]pterin

Chemical Property of 4-(cyclohexyloxy)-7-methyl-6-[1-(4-methylphenylimino)ethyl]pterin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(cyclohexyloxy)-7-methyl-6-[1-(4-methylphenylimino)ethyl]pterin

There total 3 articles about 4-(cyclohexyloxy)-7-methyl-6-[1-(4-methylphenylimino)ethyl]pterin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

6-acetyl-4-cyclohexyloxy-7-methylpterin (1254938-73-2) + p-toluidine (106-49-0,12221-03-3) → 4-(cyclohexyloxy)-7-methyl-6-[1-(4-methylphenylimino)ethyl]pterin (1254938-81-2)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 16h; Molecular sieve;

DOI:10.1515/hc-2012-0046

Reference yield:

2,6-diamino-4-(cyclohexyloxy)-5-nitrosopyrimidine (1104608-06-1) → 4-(cyclohexyloxy)-7-methyl-6-[1-(4-methylphenylimino)ethyl]pterin (1254938-81-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 14 h / Reflux

2: boron trifluoride diethyl etherate / dichloromethane / 16 h / 20 °C / Molecular sieve

With boron trifluoride diethyl etherate; In dichloromethane;

DOI:10.1515/hc-2012-0046

Reference yield:

acetylacetone (123-54-6,81235-32-7) → 4-(cyclohexyloxy)-7-methyl-6-[1-(4-methylphenylimino)ethyl]pterin (1254938-81-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 14 h / Reflux

2: boron trifluoride diethyl etherate / dichloromethane / 16 h / 20 °C / Molecular sieve

With boron trifluoride diethyl etherate; In dichloromethane;

DOI:10.1515/hc-2012-0046

upstream raw materials:

6-acetyl-4-cyclohexyloxy-7-methylpterin

p-toluidine

acetylacetone

2,6-diamino-4-(cyclohexyloxy)-5-nitrosopyrimidine