(E)-3-(3,5-Dimethoxyphenyl)-6-methoxy-2-(4-methoxyphenyl)-4-<2-(4-methoxyphenyl)ethenyl>benzofuran

Base Information

Chemical Name:(E)-3-(3,5-Dimethoxyphenyl)-6-methoxy-2-(4-methoxyphenyl)-4-<2-(4-methoxyphenyl)ethenyl>benzofuran
CAS No.:128962-14-1
Molecular Formula:C₃₃H₃₀O₆
Molecular Weight:522.598
Hs Code.:

Synonyms:(E)-3-(3,5-Dimethoxyphenyl)-6-methoxy-2-(4-methoxyphenyl)-4-<2-(4-methoxyphenyl)ethenyl>benzofuran

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Chemical Property of (E)-3-(3,5-Dimethoxyphenyl)-6-methoxy-2-(4-methoxyphenyl)-4-<2-(4-methoxyphenyl)ethenyl>benzofuran

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Technology Process of (E)-3-(3,5-Dimethoxyphenyl)-6-methoxy-2-(4-methoxyphenyl)-4-<2-(4-methoxyphenyl)ethenyl>benzofuran

There total 22 articles about (E)-3-(3,5-Dimethoxyphenyl)-6-methoxy-2-(4-methoxyphenyl)-4-<2-(4-methoxyphenyl)ethenyl>benzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1145-93-3
diethyl 4-methoxybenzylphosphonate

: 3-(3,5-dimethoxyphenyl)-6-methoxy-2-(4-methoxyphenyl)benzofuran-4-carbaldehyde

: 128962-14-1
(E)-3-(3,5-Dimethoxyphenyl)-6-methoxy-2-(4-methoxyphenyl)-4-<2-(4-methoxyphenyl)ethenyl>benzofuran

Guidance literature:: diethyl 4-methoxybenzylphosphonate; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.0833333h;

3-(3,5-dimethoxyphenyl)-6-methoxy-2-(4-methoxyphenyl)benzofuran-4-carbaldehyde; In tetrahydrofuran; at -78 - 0 ℃; for 16h;
DOI:10.1039/b901911a

Reference yield: 97.0%

: C₃₂H₂₈O₆

: 74-88-4
methyl iodide

: 128962-14-1
(E)-3-(3,5-Dimethoxyphenyl)-6-methoxy-2-(4-methoxyphenyl)-4-<2-(4-methoxyphenyl)ethenyl>benzofuran

Guidance literature:: With potassium carbonate; In acetone; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1002/adsc.201600992

Reference yield: 70.0%

: C₂₆H₂₄ClOP

: 3-(3,5-dimethoxyphenyl)-6-methoxy-2-(4-methoxyphenyl)benzofuran-4-carbaldehyde

: 128962-14-1
(E)-3-(3,5-Dimethoxyphenyl)-6-methoxy-2-(4-methoxyphenyl)-4-<2-(4-methoxyphenyl)ethenyl>benzofuran

Guidance literature:: C₂₆H₂₄ClOP; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

3-(3,5-dimethoxyphenyl)-6-methoxy-2-(4-methoxyphenyl)benzofuran-4-carbaldehyde; In tetrahydrofuran; at -78 - 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tetlet.2019.02.040