5--4-chloro-5H-1,2,3-dithiazole

Base Information

• Chemical Name: 5--4-chloro-5H-1,2,3-dithiazole
• CAS No.: 180316-20-5
• Molecular Formula: C₁₄H₁₀ClN₃S₂
• Molecular Weight: 319.839
• Mol file: 180316-20-5.mol

Synonyms:5--4-chloro-5H-1,2,3-dithiazole

Chemical Property of 5--4-chloro-5H-1,2,3-dithiazole

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 5--4-chloro-5H-1,2,3-dithiazole

There total 1 articles about 5--4-chloro-5H-1,2,3-dithiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

4,5-dichloro-1,2,3-dithiazolium chloride (75318-43-3) + N-phenyl-1,2-benzenediamine (534-85-0) → 5--4-chloro-5H-1,2,3-dithiazole (180316-20-5)

Guidance literature:

With pyridine; In tetrahydrofuran; Ambient temperature;

DOI:10.1016/0040-4039(96)00853-2

Reference yield: 93.0%

5--4-chloro-5H-1,2,3-dithiazole (180316-20-5) → 2-cyano-1-phenylbenzimidazole

Guidance literature:

With hydrogenchloride; In dichloromethane; Ambient temperature;

DOI:10.1016/0040-4039(96)00853-2

Reference yield: 72.0%

norborn-2-ene (498-66-8) + 5--4-chloro-5H-1,2,3-dithiazole (180316-20-5) → exo-3,4,5-trithiatricyclo[5.2.1.02,6]decane (23657-27-4) + 2-cyano-1-phenylbenzimidazole

Guidance literature:

at 140 - 150 ℃; for 4h; sealed tube;

DOI:10.1016/0040-4039(96)00853-2

upstream raw materials:

4,5-dichloro-1,2,3-dithiazolium chloride

N-phenyl-1,2-benzenediamine

Downstream raw materials:

exo-3,4,5-trithiatricyclo[5.2.1.0^2,6]decane

4,5-diphenyl-3,6-dihydro-1,2-dithiin