{Ni(PF₂C₆H₅)4}

Base Information

Chemical Name:{Ni(PF₂C₆H₅)4}
CAS No.:13987-00-3
Molecular Formula:C₂₄H₂₀F₈NiP₄
Molecular Weight:642.995
Hs Code.:

{Ni(PF<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)4}

Synonyms:{Ni(PF₂C₆H₅)4}

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Chemical Property of {Ni(PF₂C₆H₅)4}

Chemical Property:

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Technology Process of {Ni(PF₂C₆H₅)4}

There total 3 articles about {Ni(PF₂C₆H₅)4} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13463-39-3,71564-36-8
tetracarbonyl nickel

: 657-97-6
phenyldifluorophosphine

: 13987-00-3
{Ni(PF₂C₆H₅)4}

Guidance literature:: In neat (no solvent); byproducts: CO; mixing (Ni(CO)4) and (Ni(CO)4) at 0 °C under exclusion of air and moisture, stirring mixt. for 6 h at ambient temp., 6 h at 100 °C and 2 h at 110 °C;; removing volatile components at ambient temp. and 0.3 torr, sublimation of solid residue at 100-150 °C bath temp. and 0.1 torr;;

Reference yield:

: zinc(II) fluoride

: 15675-30-6
Ni(C₆H₅PCl₂)4

: 13987-00-3
{Ni(PF₂C₆H₅)4}

Guidance literature:: In benzene; refluxing ZnF2 and soln. of (Ni(PCl2C6H5)4) in benzene for 4 h in N2-atmosphere, stirring for 10 h at ambient temp.;; pumping off volatile components at 1 torr, dissolving residue in benzene, filtering under N2, concg. in vac., dissolving in ether, treating withactivated carbon, evapg. ether, addn. of petroleum ether, cooling with ice, recrystn., drying in vac.;;

Reference yield:

: 15675-30-6
Ni(C₆H₅PCl₂)4

: 7783-70-2
antimony pentafluoride

: 7784-35-2
arsenic(III) fluoride

: 13987-00-3
{Ni(PF₂C₆H₅)4}

Guidance literature:: In benzene; refluxing AsF3, SbF5 and soln. of (Ni(PCl2C6H5)4) in abs. benzene for 3 h with stirring (N2-atmosphere), stirring for 10 h at ambient temp.;; pumping off volatile components at 1 torr, dissolving residue in benzene, filtering under N2, concg. in vac., dissolving in ether and treating with activated carbon, evapg. ether, addn. of petroleum ether and cooling with ice, recrystn., drying in vac.;;