dimethyl 5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetyl-amino]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]-isophthalate

Base Information

Chemical Name:dimethyl 5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetyl-amino]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]-isophthalate
CAS No.:1042110-04-2
Molecular Formula:C₄₈H₆₈N₂O₁₅
Molecular Weight:913.072
Hs Code.:

dimethyl 5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetyl-amino]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]-isophthalate

Synonyms:dimethyl 5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetyl-amino]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]-isophthalate

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Chemical Property of dimethyl 5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetyl-amino]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]-isophthalate

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Technology Process of dimethyl 5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetyl-amino]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]-isophthalate

There total 6 articles about dimethyl 5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetyl-amino]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]-isophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1042109-96-5
3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetylamino]ethoxy}-ethoxy)-ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionic acid

: 99-27-4
dimethyl 5-aminoisophthalate

: 1042110-04-2
dimethyl 5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetyl-amino]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]-isophthalate

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 114971-53-8
4-iodo-2,5-dimethyl-phenol

: 1042110-04-2
dimethyl 5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetyl-amino]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]-isophthalate

Guidance literature:: Multi-step reaction with 6 steps

1.1: mesitylenemagnesium bromide / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 20 - 65 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

3.1: sodium hydroxide; water / methanol / 20 °C / Heating / reflux

3.2: pH 5

4.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 20 °C

5.1: hydrogenchloride / diethyl ether / 20 °C

6.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

With hydrogenchloride; sodium hydroxide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1042109-90-9
tert-butyl (2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetate

: 1042110-04-2
dimethyl 5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetyl-amino]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]-isophthalate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide; water / methanol / 20 °C / Heating / reflux

1.2: pH 5

2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 20 °C

3.1: hydrogenchloride / diethyl ether / 20 °C

4.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

With hydrogenchloride; sodium hydroxide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;