5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetylamino]-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]isophthalic acid

Base Information

Chemical Name:5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetylamino]-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]isophthalic acid
CAS No.:1042110-06-4
Molecular Formula:C₄₆H₆₄N₂O₁₅
Molecular Weight:885.019
Hs Code.:

5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetylamino]-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]isophthalic acid

Synonyms:5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetylamino]-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]isophthalic acid

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Chemical Property of 5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetylamino]-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]isophthalic acid

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Technology Process of 5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetylamino]-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]isophthalic acid

There total 7 articles about 5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetylamino]-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]isophthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1042110-04-2
dimethyl 5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetyl-amino]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]-isophthalate

: 1042110-06-4
5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetylamino]-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]isophthalic acid

Guidance literature:: With sodium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 3h;

Reference yield:

: 114971-53-8
4-iodo-2,5-dimethyl-phenol

: 1042110-06-4
5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetylamino]-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]isophthalic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: mesitylenemagnesium bromide / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 20 - 65 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

3.1: sodium hydroxide; water / methanol / 20 °C / Heating / reflux

3.2: pH 5

4.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 20 °C

5.1: hydrogenchloride / diethyl ether / 20 °C

6.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

7.1: sodium hydroxide; water / tetrahydrofuran / 3 h / 20 °C

With hydrogenchloride; sodium hydroxide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1042109-90-9
tert-butyl (2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetate

: 1042110-06-4
5-[3-(2-{2-[2-(2-{2-[2-(2-{2-[2-(2,5,2',4',6'-pentamethylbiphenyl-4-yloxy)acetylamino]-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)propionylamino]isophthalic acid

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide; water / methanol / 20 °C / Heating / reflux

1.2: pH 5

2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 20 °C

3.1: hydrogenchloride / diethyl ether / 20 °C

4.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C

5.1: sodium hydroxide; water / tetrahydrofuran / 3 h / 20 °C

With hydrogenchloride; sodium hydroxide; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;