Technology Process of C32H53NO6Si6
There total 5 articles about C32H53NO6Si6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tris(pentafluorophenyl)borate;
In
toluene;
at 20 ℃;
DOI:10.1021/jo2020906
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; potassium carbonate; L-proline / dimethyl sulfoxide / 2 h / 180 °C / Inert atmosphere
2: tris(pentafluorophenyl)borate / toluene / 20 °C
With
copper(l) iodide; tris(pentafluorophenyl)borate; potassium carbonate; L-proline;
In
dimethyl sulfoxide; toluene;
1: Ullmann coupling / 2: Piers-Rubinsztajn reaction;
DOI:10.1021/jo2020906
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethyl phosphite / 16 h / 160 °C / Inert atmosphere
2: copper(l) iodide; potassium carbonate; L-proline / dimethyl sulfoxide / 2 h / 180 °C / Inert atmosphere
3: tris(pentafluorophenyl)borate / toluene / 20 °C
With
copper(l) iodide; tris(pentafluorophenyl)borate; potassium carbonate; L-proline; triethyl phosphite;
In
dimethyl sulfoxide; toluene;
2: Ullmann coupling / 3: Piers-Rubinsztajn reaction;
DOI:10.1021/jo2020906