2,4,6-trimethyl-α-oxobenzeneacetonitrile

Base Information

Chemical Name:2,4,6-trimethyl-α-oxobenzeneacetonitrile
CAS No.:55878-82-5
Molecular Formula:C₁₁H₁₁NO
Molecular Weight:173.214
Hs Code.:

Synonyms:2,4,6-trimethyl-α-oxobenzeneacetonitrile

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Chemical Property of 2,4,6-trimethyl-α-oxobenzeneacetonitrile

Chemical Property:

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Technology Process of 2,4,6-trimethyl-α-oxobenzeneacetonitrile

There total 3 articles about 2,4,6-trimethyl-α-oxobenzeneacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 544-92-3
copper(I) cyanide

: 938-18-1
mesitylene-2-carboxylic acid chloride

: 55878-82-5
2,4,6-trimethyl-α-oxobenzeneacetonitrile

Guidance literature:: In toluene; acetonitrile; for 3h; Heating;

Reference yield: 40.0%

: 49685-65-6,545386-91-2
2-hydroxy-2-(2,4,6-trimethylphenyl)acetonitrile

: 487-68-3
mesytaldehyde

: 55878-82-5
2,4,6-trimethyl-α-oxobenzeneacetonitrile

Guidance literature:: With (η(6)-benzene)chloro[1,2-bis(diphenylphosphino)ethane]ruthenium(II) chloride; In benzene; at 120 ℃; for 24h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1002/adsc.201700786

Reference yield:

: 487-68-3
mesytaldehyde

: 55878-82-5
2,4,6-trimethyl-α-oxobenzeneacetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogensulfite / water; ethyl acetate / 20 h / 40 °C / Inert atmosphere; Schlenk technique; Sealed tube

2: (η(6)-benzene)chloro[1,2-bis(diphenylphosphino)ethane]ruthenium(II) chloride / benzene / 24 h / 120 °C / Inert atmosphere; Schlenk technique; Sealed tube

With (η(6)-benzene)chloro[1,2-bis(diphenylphosphino)ethane]ruthenium(II) chloride; sodium hydrogensulfite; In water; ethyl acetate; benzene;
DOI:10.1002/adsc.201700786