C₂₈H₃₃N₃O₅Si

Base Information

Chemical Name:C₂₈H₃₃N₃O₅Si
CAS No.:1229584-08-0
Molecular Formula:C₂₈H₃₃N₃O₅Si
Molecular Weight:519.673
Hs Code.:

C<sub>28</sub>H<sub>33</sub>N<sub>3</sub>O<sub>5</sub>Si

Synonyms:C₂₈H₃₃N₃O₅Si

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Chemical Property of C₂₈H₃₃N₃O₅Si

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Technology Process of C₂₈H₃₃N₃O₅Si

There total 6 articles about C₂₈H₃₃N₃O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 500-22-1
3-pyridinecarboxaldehyde

: 1229584-04-6
5-(3,4,5-trimethoxyphenyl)-1-((2-(trimethylsilyl)ethoxy)-methyl)-1H-pyrrolo[2,3-b]pyridin-2(3H)-one

: 1229584-08-0
C₂₈H₃₃N₃O₅Si

Guidance literature:: With triethylamine; In toluene; at 20 ℃; Molecular sieve;

Reference yield:

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 1229584-08-0
C₂₈H₃₃N₃O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1.25 h / 0 °C

1.2: 1.25 h

2.1: bromine; water / tert-butyl alcohol / 21.5 h / 20 °C

3.1: zinc; acetic acid / 2 h / 20 °C

4.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / acetonitrile / 2 h / 80 °C / Inert atmosphere

5.1: triethylamine / toluene / 20 °C / Molecular sieve

With water; bromine; sodium hydride; sodium carbonate; acetic acid; triethylamine; zinc; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil; tert-butyl alcohol;

Reference yield:

: 271-63-6
7-Azaindole

: 1229584-08-0
C₂₈H₃₃N₃O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1.25 h / 0 °C

1.2: 1.25 h

2.1: bromine; water / tert-butyl alcohol / 21.5 h / 20 °C

3.1: zinc; acetic acid / 2 h / 20 °C

4.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / acetonitrile / 2 h / 80 °C / Inert atmosphere

5.1: triethylamine / toluene / 20 °C / Molecular sieve

With water; bromine; sodium hydride; sodium carbonate; acetic acid; triethylamine; zinc; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil; tert-butyl alcohol;