3-iodo-4,5-diethoxybenzaldehyde

Base Information

Chemical Name:3-iodo-4,5-diethoxybenzaldehyde
CAS No.:443291-33-6
Molecular Formula:C₁₁H₁₃IO₃
Molecular Weight:320.127
Hs Code.:

Synonyms:3-iodo-4,5-diethoxybenzaldehyde

Suppliers and Price of 3-iodo-4,5-diethoxybenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 2 raw suppliers

Chemical Property of 3-iodo-4,5-diethoxybenzaldehyde

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

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Technology Process of 3-iodo-4,5-diethoxybenzaldehyde

There total 2 articles about 3-iodo-4,5-diethoxybenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 54246-05-8
3-iodo-4,5-dihydroxybenzaldehyde

: 75-03-6
ethyl iodide

: 443291-33-6
3-iodo-4,5-diethoxybenzaldehyde

Guidance literature:: 3-iodo-4,5-dihydroxybenzaldehyde; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 20 ℃; for 0.583333h; Inert atmosphere;

ethyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1080/00304948.2012.643700

Reference yield:

: 5438-36-8
5-iodovaniline

: 443291-33-6
3-iodo-4,5-diethoxybenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine; aluminum (III) chloride / dichloromethane / 16.33 h / 50 °C / Inert atmosphere; Reflux

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.58 h / 20 °C / Inert atmosphere

2.2: 0.5 h / 20 °C / Inert atmosphere

With pyridine; aluminum (III) chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/00304948.2012.643700

Reference yield:

: 443291-33-6
3-iodo-4,5-diethoxybenzaldehyde

: 5-(3,4-diethoxy-5-iodobenzyl)pyrimidine-2,4-diamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / dimethyl sulfoxide / 65 - 90 °C / Inert atmosphere

1.2: 1.08 h / 90 °C / Inert atmosphere

2.1: sodium methylate; aniline hydrochloride / ethanol / 1 h / 78 °C / Inert atmosphere

2.2: 4 h / 78 °C / Inert atmosphere

With sodium methylate; aniline hydrochloride; In ethanol; dimethyl sulfoxide;
DOI:10.1016/j.bmc.2014.11.009