2-[5-(2,2-dimethyl-propionyloxy)-2-methoxycarbonylamino-phenyl]-2-phenylsulfanyl-propionic acid

Base Information

Chemical Name:2-[5-(2,2-dimethyl-propionyloxy)-2-methoxycarbonylamino-phenyl]-2-phenylsulfanyl-propionic acid
CAS No.:354116-70-4
Molecular Formula:C₂₂H₂₅NO₆S
Molecular Weight:431.51
Hs Code.:

Synonyms:2-[5-(2,2-dimethyl-propionyloxy)-2-methoxycarbonylamino-phenyl]-2-phenylsulfanyl-propionic acid

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Chemical Property of 2-[5-(2,2-dimethyl-propionyloxy)-2-methoxycarbonylamino-phenyl]-2-phenylsulfanyl-propionic acid

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Technology Process of 2-[5-(2,2-dimethyl-propionyloxy)-2-methoxycarbonylamino-phenyl]-2-phenylsulfanyl-propionic acid

There total 5 articles about 2-[5-(2,2-dimethyl-propionyloxy)-2-methoxycarbonylamino-phenyl]-2-phenylsulfanyl-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 354116-65-7
C-methoxy-N-(4'-trimethylacetyloxyphenyl)-O-(2-phenylsulfanylpropanoyl)hydroxamic acid

: 354116-70-4
2-[5-(2,2-dimethyl-propionyloxy)-2-methoxycarbonylamino-phenyl]-2-phenylsulfanyl-propionic acid

Guidance literature:: With potassium hexamethylsilazane; In tetrahydrofuran; at -80 - 20 ℃; for 13h;
DOI:10.3987/com-01-9177

Reference yield:

: 17431-94-6
2-phenylsulfanyl-propionic acid

: 354116-70-4
2-[5-(2,2-dimethyl-propionyloxy)-2-methoxycarbonylamino-phenyl]-2-phenylsulfanyl-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / DCC; DMAP / CH₂Cl₂ / 4 h / 20 °C

2: 70 percent / KHMDS / tetrahydrofuran / 13 h / -80 - 20 °C

With dmap; potassium hexamethylsilazane; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;
DOI:10.3987/com-01-9177

Reference yield:

: 4195-17-9
4-nitrophenyl pivalate

: 354116-70-4
2-[5-(2,2-dimethyl-propionyloxy)-2-methoxycarbonylamino-phenyl]-2-phenylsulfanyl-propionic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 30 percent / Zn; NH₄Cl / ethanol; H₂O / 1.5 h / 60 °C

2: 88 percent / NaHCO₃ / diethyl ether / 1.5 h / 20 °C

3: 87 percent / DCC; DMAP / CH₂Cl₂ / 4 h / 20 °C

4: 70 percent / KHMDS / tetrahydrofuran / 13 h / -80 - 20 °C

With dmap; potassium hexamethylsilazane; sodium hydrogencarbonate; ammonium chloride; dicyclohexyl-carbodiimide; zinc; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water;
DOI:10.3987/com-01-9177