C-methoxy-N-(4'-trimethylacetyloxyphenyl)-O-(2-phenylsulfanylpropanoyl)hydroxamic acid

Base Information

Chemical Name:C-methoxy-N-(4'-trimethylacetyloxyphenyl)-O-(2-phenylsulfanylpropanoyl)hydroxamic acid
CAS No.:354116-65-7
Molecular Formula:C₂₂H₂₅NO₆S
Molecular Weight:431.51
Hs Code.:

Synonyms:C-methoxy-N-(4'-trimethylacetyloxyphenyl)-O-(2-phenylsulfanylpropanoyl)hydroxamic acid

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Chemical Property of C-methoxy-N-(4'-trimethylacetyloxyphenyl)-O-(2-phenylsulfanylpropanoyl)hydroxamic acid

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Technology Process of C-methoxy-N-(4'-trimethylacetyloxyphenyl)-O-(2-phenylsulfanylpropanoyl)hydroxamic acid

There total 3 articles about C-methoxy-N-(4'-trimethylacetyloxyphenyl)-O-(2-phenylsulfanylpropanoyl)hydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 17431-94-6
2-phenylsulfanyl-propionic acid

: 354116-64-6
C-methoxy-N-(4-trimethylacetyloxyphenyl)hydroxamic acid

: 354116-65-7
C-methoxy-N-(4'-trimethylacetyloxyphenyl)-O-(2-phenylsulfanylpropanoyl)hydroxamic acid

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 4h;
DOI:10.3987/com-01-9177

Reference yield:

: 4195-17-9
4-nitrophenyl pivalate

: 354116-65-7
C-methoxy-N-(4'-trimethylacetyloxyphenyl)-O-(2-phenylsulfanylpropanoyl)hydroxamic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 30 percent / Zn; NH₄Cl / ethanol; H₂O / 1.5 h / 60 °C

2: 88 percent / NaHCO₃ / diethyl ether / 1.5 h / 20 °C

3: 87 percent / DCC; DMAP / CH₂Cl₂ / 4 h / 20 °C

With dmap; sodium hydrogencarbonate; ammonium chloride; dicyclohexyl-carbodiimide; zinc; In diethyl ether; ethanol; dichloromethane; water;
DOI:10.3987/com-01-9177

Reference yield:

: N-(4-trimethylacetyloxyphenyl)hydroxylamine

: 354116-65-7
C-methoxy-N-(4'-trimethylacetyloxyphenyl)-O-(2-phenylsulfanylpropanoyl)hydroxamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / NaHCO₃ / diethyl ether / 1.5 h / 20 °C

2: 87 percent / DCC; DMAP / CH₂Cl₂ / 4 h / 20 °C

With dmap; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane;
DOI:10.3987/com-01-9177