2-Benzoyl-3-<<(tert-butyl)dimethylsilyl>oxy>-3,6-dihydro-2H-1,2-oxazine

Base Information

Chemical Name:2-Benzoyl-3-<<(tert-butyl)dimethylsilyl>oxy>-3,6-dihydro-2H-1,2-oxazine
CAS No.:131507-59-0
Molecular Formula:C₁₇H₂₅NO₃Si
Molecular Weight:319.476
Hs Code.:

Synonyms:2-Benzoyl-3-<<(tert-butyl)dimethylsilyl>oxy>-3,6-dihydro-2H-1,2-oxazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Benzoyl-3-<<(tert-butyl)dimethylsilyl>oxy>-3,6-dihydro-2H-1,2-oxazine

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Technology Process of 2-Benzoyl-3-<<(tert-butyl)dimethylsilyl>oxy>-3,6-dihydro-2H-1,2-oxazine

There total 3 articles about 2-Benzoyl-3-<<(tert-butyl)dimethylsilyl>oxy>-3,6-dihydro-2H-1,2-oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 495-18-1
Benzohydroxamic acid

: 109987-02-2,88346-87-6
trans-1-(tert-butyldimethylsiloxy)butadiene

: 131507-59-0
2-Benzoyl-3-<<(tert-butyl)dimethylsilyl>oxy>-3,6-dihydro-2H-1,2-oxazine

: 131507-54-5
2-Benzoyl-6-<<(tert-butyl)dimethylsilyl>oxy>-3,6-dihydro-2H-1,2-oxazine

Guidance literature:: With molecular sieve; tetrapropylammonium periodate; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1002/hlca.19910740806

Reference yield:

: 98-88-4
benzoyl chloride

: 131507-59-0
2-Benzoyl-3-<<(tert-butyl)dimethylsilyl>oxy>-3,6-dihydro-2H-1,2-oxazine

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / NH₂OH*HCl, K₂CO₃ / diethyl ether; H₂O / Ambient temperature

2: 6 percent / (Pr₄N)IO₄, molecular sieves / CH₂Cl₂ / 1 h / 0 °C

With molecular sieve; tetrapropylammonium periodate; hydroxylamine hydrochloride; potassium carbonate; In diethyl ether; dichloromethane; water;
DOI:10.1002/hlca.19910740806

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 131507-59-0
2-Benzoyl-3-<<(tert-butyl)dimethylsilyl>oxy>-3,6-dihydro-2H-1,2-oxazine

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / Et₃N, NaI / acetonitrile / 7 h / 50 °C

2: 6 percent / (Pr₄N)IO₄, molecular sieves / CH₂Cl₂ / 1 h / 0 °C

With molecular sieve; tetrapropylammonium periodate; triethylamine; sodium iodide; In dichloromethane; acetonitrile;
DOI:10.1002/hlca.19910740806