(E,E)-6-<<<<4-<(4-hexylphenyl)sulfonyl>-1,3-butadienyl>amino>carbonyl>oxy>-N,N,N-trimethyl-1-hexanaminium bromide

Base Information

Chemical Name:(E,E)-6-<<<<4-<(4-hexylphenyl)sulfonyl>-1,3-butadienyl>amino>carbonyl>oxy>-N,N,N-trimethyl-1-hexanaminium bromide
CAS No.:131906-60-0
Molecular Formula:Br*C₂₆H₄₃N₂O₄S
Molecular Weight:559.608
Hs Code.:

Synonyms:(E,E)-6-<<<<4-<(4-hexylphenyl)sulfonyl>-1,3-butadienyl>amino>carbonyl>oxy>-N,N,N-trimethyl-1-hexanaminium bromide

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Chemical Property of (E,E)-6-<<<<4-<(4-hexylphenyl)sulfonyl>-1,3-butadienyl>amino>carbonyl>oxy>-N,N,N-trimethyl-1-hexanaminium bromide

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Technology Process of (E,E)-6-<<<<4-<(4-hexylphenyl)sulfonyl>-1,3-butadienyl>amino>carbonyl>oxy>-N,N,N-trimethyl-1-hexanaminium bromide

There total 6 articles about (E,E)-6-<<<<4-<(4-hexylphenyl)sulfonyl>-1,3-butadienyl>amino>carbonyl>oxy>-N,N,N-trimethyl-1-hexanaminium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 131932-55-3
6-bromohexyl ((E,E)-4-<(4-hexylphenyl)sulfonyl>-1,3-butadienyl)carbamate

: 75-50-3
trimethylamine

: 131906-60-0
(E,E)-6-<<<<4-<(4-hexylphenyl)sulfonyl>-1,3-butadienyl>amino>carbonyl>oxy>-N,N,N-trimethyl-1-hexanaminium bromide

Guidance literature:: In methanol; at 4 ℃; for 72h;
DOI:10.1021/jo00007a041

Reference yield:

: 4286-55-9
1-bromo-6-hexanol

: 131906-60-0
(E,E)-6-<<<<4-<(4-hexylphenyl)sulfonyl>-1,3-butadienyl>amino>carbonyl>oxy>-N,N,N-trimethyl-1-hexanaminium bromide

Guidance literature:: Multi-step reaction with 4 steps

1: 4-tert-butylcatechol / toluene / 0.25 h / Heating

2: 43 percent / (i-Pr)2NEt / tetrahydrofuran / 1.) -78 deg C, 30 min, 2.) gradually warming

3: 82 percent / 85 percent m-ClC₆H₄CO₃H / CH₂Cl₂ / -15 deg C -> 25 deg C

4: 69 percent / methanol / 72 h / 4 °C

With 4-tert-Butylcatechol; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/jo00007a041

Reference yield:

: 4619-85-6
4-hexylbenzenethiol

: 131906-60-0
(E,E)-6-<<<<4-<(4-hexylphenyl)sulfonyl>-1,3-butadienyl>amino>carbonyl>oxy>-N,N,N-trimethyl-1-hexanaminium bromide

Guidance literature:: Multi-step reaction with 4 steps

1: 1.35 M Cl₂ / CCl₄ / 0.33 h / 0 °C

2: 43 percent / (i-Pr)2NEt / tetrahydrofuran / 1.) -78 deg C, 30 min, 2.) gradually warming

3: 82 percent / 85 percent m-ClC₆H₄CO₃H / CH₂Cl₂ / -15 deg C -> 25 deg C

4: 69 percent / methanol / 72 h / 4 °C

With chlorine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane;
DOI:10.1021/jo00007a041