6-O-(1'-ethoxyethyl)-1,2-O-isopropylidene-4,5,6-tri-O-(N-phenylcarbamoyl)-myo-inositol

Base Information

Chemical Name:6-O-(1'-ethoxyethyl)-1,2-O-isopropylidene-4,5,6-tri-O-(N-phenylcarbamoyl)-myo-inositol
CAS No.:194786-37-3
Molecular Formula:C₃₄H₃₉N₃O₁₀
Molecular Weight:649.698
Hs Code.:

Synonyms:6-O-(1'-ethoxyethyl)-1,2-O-isopropylidene-4,5,6-tri-O-(N-phenylcarbamoyl)-myo-inositol

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Chemical Property of 6-O-(1'-ethoxyethyl)-1,2-O-isopropylidene-4,5,6-tri-O-(N-phenylcarbamoyl)-myo-inositol

Chemical Property:

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Technology Process of 6-O-(1'-ethoxyethyl)-1,2-O-isopropylidene-4,5,6-tri-O-(N-phenylcarbamoyl)-myo-inositol

There total 5 articles about 6-O-(1'-ethoxyethyl)-1,2-O-isopropylidene-4,5,6-tri-O-(N-phenylcarbamoyl)-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 109-92-2,25104-37-4
ethyl vinyl ether

: 194786-36-2
(+)-D-1,2-O-isopropylidene-3,4,5-tri-O-(N-phenylcarbamoyl)-myo-inositol

: 194786-37-3
6-O-(1'-ethoxyethyl)-1,2-O-isopropylidene-4,5,6-tri-O-(N-phenylcarbamoyl)-myo-inositol

Guidance literature:: With acetic acid; In N,N-dimethyl-formamide; for 2h; Ambient temperature;
DOI:10.1016/S0008-6215(97)00131-6

Reference yield:

: phytic acid

: 194786-37-3
6-O-(1'-ethoxyethyl)-1,2-O-isopropylidene-4,5,6-tri-O-(N-phenylcarbamoyl)-myo-inositol

Guidance literature:: Multi-step reaction with 5 steps

1: NaOAc, Baker's yeast / H₂O / 7 h / 45 °C

2: DMAP, DIPEA / CH₂Cl₂ / 48 h / Ambient temperature

3: 48 percent / formic acid, sodium formate, NaOH / H₂O / 31 h / Heating

4: 90 percent / PhSO₃H / acetonitrile; tetrahydrofuran / 2 h

5: 97 percent / AcOH / dimethylformamide / 2 h / Ambient temperature

With dmap; sodium hydroxide; formic acid; baker's yeast; sodium formate; sodium acetate; acetic acid; N-ethyl-N,N-diisopropylamine; benzenesulfonic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0008-6215(97)00131-6

Reference yield:

: 172219-04-4
(+)-D-3,4,5-tri-O-phenylcarbamoyl myo-inositol

: 194786-37-3
6-O-(1'-ethoxyethyl)-1,2-O-isopropylidene-4,5,6-tri-O-(N-phenylcarbamoyl)-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / PhSO₃H / acetonitrile; tetrahydrofuran / 2 h

2: 97 percent / AcOH / dimethylformamide / 2 h / Ambient temperature

With acetic acid; benzenesulfonic acid; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0008-6215(97)00131-6