(+)-D-1,2-O-isopropylidene-3,4,5-tri-O-(N-phenylcarbamoyl)-myo-inositol

Base Information

Chemical Name:(+)-D-1,2-O-isopropylidene-3,4,5-tri-O-(N-phenylcarbamoyl)-myo-inositol
CAS No.:194786-36-2
Molecular Formula:C₃₀H₃₁N₃O₉
Molecular Weight:577.591
Hs Code.:

Synonyms:(+)-D-1,2-O-isopropylidene-3,4,5-tri-O-(N-phenylcarbamoyl)-myo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-D-1,2-O-isopropylidene-3,4,5-tri-O-(N-phenylcarbamoyl)-myo-inositol

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

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Technology Process of (+)-D-1,2-O-isopropylidene-3,4,5-tri-O-(N-phenylcarbamoyl)-myo-inositol

There total 4 articles about (+)-D-1,2-O-isopropylidene-3,4,5-tri-O-(N-phenylcarbamoyl)-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 77-76-9
2,2-dimethoxy-propane

: 172219-04-4
(+)-D-3,4,5-tri-O-phenylcarbamoyl myo-inositol

: 194786-36-2
(+)-D-1,2-O-isopropylidene-3,4,5-tri-O-(N-phenylcarbamoyl)-myo-inositol

Guidance literature:: With benzenesulfonic acid; In tetrahydrofuran; acetonitrile; for 2h;
DOI:10.1016/S0008-6215(97)00131-6

Reference yield:

: phytic acid

: 194786-36-2
(+)-D-1,2-O-isopropylidene-3,4,5-tri-O-(N-phenylcarbamoyl)-myo-inositol

Guidance literature:: Multi-step reaction with 4 steps

1: NaOAc, Baker's yeast / H₂O / 7 h / 45 °C

2: DMAP, DIPEA / CH₂Cl₂ / 48 h / Ambient temperature

3: 48 percent / formic acid, sodium formate, NaOH / H₂O / 31 h / Heating

4: 90 percent / PhSO₃H / acetonitrile; tetrahydrofuran / 2 h

With dmap; sodium hydroxide; formic acid; baker's yeast; sodium formate; sodium acetate; N-ethyl-N,N-diisopropylamine; benzenesulfonic acid; In tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1016/S0008-6215(97)00131-6

Reference yield:

: 166660-36-2
(+)-D-3,4,5-tri-O-(N-phenylcarbamoyl)-myo-inositol-1,2,3-tris(phosphate)

: 194786-36-2
(+)-D-1,2-O-isopropylidene-3,4,5-tri-O-(N-phenylcarbamoyl)-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / formic acid, sodium formate, NaOH / H₂O / 31 h / Heating

2: 90 percent / PhSO₃H / acetonitrile; tetrahydrofuran / 2 h

With sodium hydroxide; formic acid; sodium formate; benzenesulfonic acid; In tetrahydrofuran; water; acetonitrile;
DOI:10.1016/S0008-6215(97)00131-6