4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(4-(4-ethoxy-3-(5-methyl-4-oxo-7-propyl-1,4-dihydroimidazo[1,5-f][1,2,4]triazin-2-yl)phenylsulfonyl)piperazin-1-yl)acetate

Base Information

Chemical Name:4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(4-(4-ethoxy-3-(5-methyl-4-oxo-7-propyl-1,4-dihydroimidazo[1,5-f][1,2,4]triazin-2-yl)phenylsulfonyl)piperazin-1-yl)acetate
CAS No.:1134191-22-2
Molecular Formula:C₃₂H₃₄N₆O₆S₄
Molecular Weight:726.923
Hs Code.:

4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(4-(4-ethoxy-3-(5-methyl-4-oxo-7-propyl-1,4-dihydroimidazo[1,5-f][1,2,4]triazin-2-yl)phenylsulfonyl)piperazin-1-yl)acetate

Synonyms:4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(4-(4-ethoxy-3-(5-methyl-4-oxo-7-propyl-1,4-dihydroimidazo[1,5-f][1,2,4]triazin-2-yl)phenylsulfonyl)piperazin-1-yl)acetate

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Chemical Property of 4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(4-(4-ethoxy-3-(5-methyl-4-oxo-7-propyl-1,4-dihydroimidazo[1,5-f][1,2,4]triazin-2-yl)phenylsulfonyl)piperazin-1-yl)acetate

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Technology Process of 4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(4-(4-ethoxy-3-(5-methyl-4-oxo-7-propyl-1,4-dihydroimidazo[1,5-f][1,2,4]triazin-2-yl)phenylsulfonyl)piperazin-1-yl)acetate

There total 11 articles about 4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(4-(4-ethoxy-3-(5-methyl-4-oxo-7-propyl-1,4-dihydroimidazo[1,5-f][1,2,4]triazin-2-yl)phenylsulfonyl)piperazin-1-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18274-81-2
desmethyl anethole trithione

: 1134191-27-7
2-(4-(4-ethoxy-3-(5-methyl-4-oxo-7-propyl-1,4-dihydroimidazo[1,5-f][1,2,4]triazin-2-yl)phenylsulfonyl)piperazin-1-yl)acetic acid

: 1134191-22-2
4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(4-(4-ethoxy-3-(5-methyl-4-oxo-7-propyl-1,4-dihydroimidazo[1,5-f][1,2,4]triazin-2-yl)phenylsulfonyl)piperazin-1-yl)acetate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 5h;

Reference yield:

: 6609-57-0
2-ethoxybenzonitrile

: 1134191-22-2
4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(4-(4-ethoxy-3-(5-methyl-4-oxo-7-propyl-1,4-dihydroimidazo[1,5-f][1,2,4]triazin-2-yl)phenylsulfonyl)piperazin-1-yl)acetate

Guidance literature:: Multi-step reaction with 7 steps

1.1: trimethylaluminum; ammonium chloride / toluene / 9.5 h / 0 - 20 °C / Heating / reflux

2.1: hydrazine / methanol / 0.17 h / 0 °C

2.2: 4 h / Heating / reflux

3.1: trichlorophosphate / acetic acid / 2 h / 110 °C

4.1: chlorosulfonic acid / dichloromethane / 3 h / 20 °C

5.1: triethylamine / dichloromethane / 3 h / 20 °C

6.1: sodium hydroxide; water / ethanol / 2 h / 90 °C

6.2: pH 2.3

7.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 5 h / 20 °C

With chlorosulfonic acid; dmap; sodium hydroxide; water; trimethylaluminum; ammonium chloride; triethylamine; dicyclohexyl-carbodiimide; hydrazine; trichlorophosphate; In methanol; ethanol; dichloromethane; acetic acid; toluene;

Reference yield:

: 18637-00-8
2-ethoxy-benzamidine hydrochloride

: 1134191-22-2
4-(5-thioxo-5H-1,2-dithiol-3-yl)phenyl 2-(4-(4-ethoxy-3-(5-methyl-4-oxo-7-propyl-1,4-dihydroimidazo[1,5-f][1,2,4]triazin-2-yl)phenylsulfonyl)piperazin-1-yl)acetate

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrazine / methanol / 0.17 h / 0 °C

1.2: 4 h / Heating / reflux

2.1: trichlorophosphate / acetic acid / 2 h / 110 °C

3.1: chlorosulfonic acid / dichloromethane / 3 h / 20 °C

4.1: triethylamine / dichloromethane / 3 h / 20 °C

5.1: sodium hydroxide; water / ethanol / 2 h / 90 °C

5.2: pH 2.3

6.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 5 h / 20 °C

With chlorosulfonic acid; dmap; sodium hydroxide; water; triethylamine; dicyclohexyl-carbodiimide; hydrazine; trichlorophosphate; In methanol; ethanol; dichloromethane; acetic acid;