methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-tridesoxy-α-D-ribohexopyranoside

Base Information

Chemical Name:methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-tridesoxy-α-D-ribohexopyranoside
CAS No.:75412-25-8
Molecular Formula:C₁₄H₁₆BrN₃O₄
Molecular Weight:370.203
Hs Code.:

Synonyms:methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-tridesoxy-α-D-ribohexopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-tridesoxy-α-D-ribohexopyranoside

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Technology Process of methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-tridesoxy-α-D-ribohexopyranoside

There total 1 articles about methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-tridesoxy-α-D-ribohexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 16848-77-4
(4aR,6S,8S,8aS)-8-Azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine

: 75412-25-8
methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-tridesoxy-α-D-ribohexopyranoside

Guidance literature:: With N-Bromosuccinimide; carbonate de baryum; In tetrachloromethane; for 2.5h; Heating;
DOI:10.1016/0040-4020(81)85015-6

Reference yield: 80.0%

: 75412-25-8
methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-tridesoxy-α-D-ribohexopyranoside

: 100-51-6,185532-71-2
benzyl alcohol

: 75412-35-0
benzyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-tridesoxy-β-D-ribo-hexopyranoside

: benzyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-tridesoxy-α-D-ribo-hexopyranoside

Guidance literature:: With acide p-toluene-sulfonique; In hexane; at 20 ℃; for 20h; Heating;
DOI:10.1016/0040-4020(81)85015-6

Reference yield:

: 75412-25-8
methyl 3-azido-4-O-benzoyl-6-bromo-2,3,6-tridesoxy-α-D-ribohexopyranoside

: Acetic acid (2S,3R,4S,6S)-4-acetoxy-6-((3S,4S,6S)-4-amino-6-benzyloxy-2-methylene-tetrahydro-pyran-3-yloxy)-2-methyl-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 5 steps

1: acide p-toluene-sulfonique / hexane / 20 h / 20 °C / Heating

2: 77 percent / 0.1M methanolate de sodium / methanol / 3 h / 20 °C

3: 10.3 g / acide p-toluenesulfonique / benzene / 2.5 h / 20 °C

4: 30 percent / fluorure d'argent, pyridine / 168 h / 20 °C

5: H₂ / nickel de Raney / methanol / 15 h / 1 Torr

With pyridine; acide p-toluene-sulfonique; acide p-toluenesulfonique; hydrogen; sodium methylate; silver fluoride; nickel de Raney; In methanol; hexane; benzene;
DOI:10.1016/0040-4020(81)85015-6