benzyl 4-O-(3,4-di-O-acetyl-2,6-didesoxy-α-L-lyxo-hexopyranosyl)-3-azido-2,3,6-tridesoxy-α-D-erythro-hex-5-enopyranoside

Base Information

Chemical Name:benzyl 4-O-(3,4-di-O-acetyl-2,6-didesoxy-α-L-lyxo-hexopyranosyl)-3-azido-2,3,6-tridesoxy-α-D-erythro-hex-5-enopyranoside
CAS No.:75412-38-3
Molecular Formula:C₂₃H₂₉N₃O₈
Molecular Weight:475.499
Hs Code.:

Synonyms:benzyl 4-O-(3,4-di-O-acetyl-2,6-didesoxy-α-L-lyxo-hexopyranosyl)-3-azido-2,3,6-tridesoxy-α-D-erythro-hex-5-enopyranoside

Suppliers and Price of benzyl 4-O-(3,4-di-O-acetyl-2,6-didesoxy-α-L-lyxo-hexopyranosyl)-3-azido-2,3,6-tridesoxy-α-D-erythro-hex-5-enopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 4-O-(3,4-di-O-acetyl-2,6-didesoxy-α-L-lyxo-hexopyranosyl)-3-azido-2,3,6-tridesoxy-α-D-erythro-hex-5-enopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 4-O-(3,4-di-O-acetyl-2,6-didesoxy-α-L-lyxo-hexopyranosyl)-3-azido-2,3,6-tridesoxy-α-D-erythro-hex-5-enopyranoside

There total 22 articles about benzyl 4-O-(3,4-di-O-acetyl-2,6-didesoxy-α-L-lyxo-hexopyranosyl)-3-azido-2,3,6-tridesoxy-α-D-erythro-hex-5-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 75412-37-2
benzyl 4-O-(3,4-di-O-acetyl-2,6-didesoxy-α-L-lyxo-hexopyranosyl)-3-azido-6-bromo-2,3,6-tridesoxy-α-D-ribo-hexopyranoside

: 75412-38-3
benzyl 4-O-(3,4-di-O-acetyl-2,6-didesoxy-α-L-lyxo-hexopyranosyl)-3-azido-2,3,6-tridesoxy-α-D-erythro-hex-5-enopyranoside

Guidance literature:: With pyridine; silver fluoride; at 20 ℃; for 168h;
DOI:10.1016/0040-4020(81)85015-6

Reference yield: 30.0%

: Acetic acid (2S,3S,4S,6S)-3-acetoxy-6-((2S,3S,4S,6S)-4-azido-6-benzyloxy-2-bromomethyl-tetrahydro-pyran-3-yloxy)-2-methyl-tetrahydro-pyran-4-yl ester

: 75412-38-3
benzyl 4-O-(3,4-di-O-acetyl-2,6-didesoxy-α-L-lyxo-hexopyranosyl)-3-azido-2,3,6-tridesoxy-α-D-erythro-hex-5-enopyranoside

Guidance literature:: With silver fluoride;
DOI:10.1016/S0040-4039(00)93163-0

Reference yield:

: 16848-77-4
(4aR,6S,8S,8aS)-8-Azido-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxine

: 75412-38-3
benzyl 4-O-(3,4-di-O-acetyl-2,6-didesoxy-α-L-lyxo-hexopyranosyl)-3-azido-2,3,6-tridesoxy-α-D-erythro-hex-5-enopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / carbonate de baryum, N-bromosuccinimide / CCl₄ / 2.5 h / Heating

2: acide p-toluene-sulfonique / hexane / 20 h / 20 °C / Heating

3: 77 percent / 0.1M methanolate de sodium / methanol / 3 h / 20 °C

4: 10.3 g / acide p-toluenesulfonique / benzene / 2.5 h / 20 °C

5: 30 percent / fluorure d'argent, pyridine / 168 h / 20 °C

With pyridine; N-Bromosuccinimide; acide p-toluene-sulfonique; acide p-toluenesulfonique; carbonate de baryum; sodium methylate; silver fluoride; In methanol; tetrachloromethane; hexane; benzene;
DOI:10.1016/0040-4020(81)85015-6