2,2-dimethyl-3-phenyl-1-propyl p-methoxybenzenesulfonate

Base Information

• Chemical Name: 2,2-dimethyl-3-phenyl-1-propyl p-methoxybenzenesulfonate
• CAS No.: 524698-46-2
• Molecular Formula: C₁₈H₂₂O₄S
• Molecular Weight: 334.436
• Mol file: 524698-46-2.mol

Synonyms:2,2-dimethyl-3-phenyl-1-propyl p-methoxybenzenesulfonate

Chemical Property of 2,2-dimethyl-3-phenyl-1-propyl p-methoxybenzenesulfonate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2,2-dimethyl-3-phenyl-1-propyl p-methoxybenzenesulfonate

There total 1 articles about 2,2-dimethyl-3-phenyl-1-propyl p-methoxybenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2,2-dimethyl-3-phenyl-1-propanol (13351-61-6) + 4-methoxy-phenyl-sulphonyl chloride (98-68-0) → 2,2-dimethyl-3-phenyl-1-propyl p-methoxybenzenesulfonate (524698-46-2)

Guidance literature:

With pyridine; In chloroform; at 20 ℃; for 12h;

DOI:10.1021/jo026449n

Reference yield: 62.0%

phenylmagnesium bromide + 2,2-dimethyl-3-phenyl-1-propyl p-methoxybenzenesulfonate (524698-46-2) → [1,1';4',1'']terphenyl (92-94-4,94363-13-0) + 4-methoxylbiphenyl (613-37-6)

Guidance literature:

[1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride; In tetrahydrofuran; for 28h; Heating;

DOI:10.1021/jo026449n

Reference yield: 60.0%

para-methylphenylmagnesium bromide (4294-57-9) + 2,2-dimethyl-3-phenyl-1-propyl p-methoxybenzenesulfonate (524698-46-2) → 4-(4-tolyl)anisole (53040-92-9) + 1,4-bis(p-tolyl)benzene (97295-31-3)

Guidance literature:

[1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride; In tetrahydrofuran; for 28h; Heating;

DOI:10.1021/jo026449n

upstream raw materials:

2,2-dimethyl-3-phenyl-1-propanol

4-methoxy-phenyl-sulphonyl chloride

Downstream raw materials:

[1,1';4',1'']terphenyl

4-methoxylbiphenyl

4-(4-tolyl)anisole

1,4-bis(p-tolyl)benzene

Refernces