2-(2-chlorophenoxy)-5-hexylphenol

Base Information

Chemical Name:2-(2-chlorophenoxy)-5-hexylphenol
CAS No.:1574496-70-0
Molecular Formula:C₁₈H₂₁ClO₂
Molecular Weight:304.817
Hs Code.:

Synonyms:2-(2-chlorophenoxy)-5-hexylphenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-chlorophenoxy)-5-hexylphenol

Chemical Property:

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Technology Process of 2-(2-chlorophenoxy)-5-hexylphenol

There total 7 articles about 2-(2-chlorophenoxy)-5-hexylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1606161-80-1
1-(2-chlorophenoxy)-4-hexyl-2-methoxybenzene

: 1574496-70-0
2-(2-chlorophenoxy)-5-hexylphenol

Guidance literature:: 1-(2-chlorophenoxy)-4-hexyl-2-methoxybenzene; With boron tribromide; In dichloromethane; at 20 ℃; Cooling;

With methanol; at -40 ℃; Cooling;
DOI:10.1002/cmdc.201300429

Reference yield:

: 2426-87-1
3-methoxy-4-(phenylmethoxy)benzaldehyde

: 1574496-70-0
2-(2-chlorophenoxy)-5-hexylphenol

Guidance literature:: Multi-step reaction with 6 steps

1.1: pentyltriphenylphosphonium bromide / cyclohexane; tetrahydrofuran / 0.5 h / -78 °C

1.2: 2 h / Cooling

2.1: palladium on activated charcoal; hydrogen / ethanol / 6 h / 760.05 Torr

3.1: 18-crown-6 ether / N,N-dimethyl-formamide / 3 h / 110 °C / Inert atmosphere

4.1: palladium on activated charcoal; hydrogen / ethanol / 6 h / 760.05 Torr

5.1: copper(l) chloride; acetic acid; sodium nitrite / water / 2 h / Cooling with ice

6.1: boron tribromide / dichloromethane / 20 °C / Cooling

6.2: -40 °C / Cooling

With 18-crown-6 ether; palladium on activated charcoal; pentyltriphenylphosphonium bromide; hydrogen; boron tribromide; acetic acid; copper(l) chloride; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201300429

Reference yield:

: 1606161-76-5
1-(benzyloxy)-4-(hex-1-en-1-yl)-2-methoxybenzene

: 1574496-70-0
2-(2-chlorophenoxy)-5-hexylphenol

Guidance literature:: Multi-step reaction with 5 steps

1.1: palladium on activated charcoal; hydrogen / ethanol / 6 h / 760.05 Torr

2.1: 18-crown-6 ether / N,N-dimethyl-formamide / 3 h / 110 °C / Inert atmosphere

3.1: palladium on activated charcoal; hydrogen / ethanol / 6 h / 760.05 Torr

4.1: copper(l) chloride; acetic acid; sodium nitrite / water / 2 h / Cooling with ice

5.1: boron tribromide / dichloromethane / 20 °C / Cooling

5.2: -40 °C / Cooling

With 18-crown-6 ether; palladium on activated charcoal; hydrogen; boron tribromide; acetic acid; copper(l) chloride; sodium nitrite; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201300429