Carbonic acid adamantan-1-yl ester 4-[bis-(2-iodo-ethyl)-amino]-phenyl ester

Base Information

Chemical Name:Carbonic acid adamantan-1-yl ester 4-[bis-(2-iodo-ethyl)-amino]-phenyl ester
CAS No.:172973-93-2
Molecular Formula:C₂₁H₂₇I₂NO₃
Molecular Weight:595.259
Hs Code.:

Synonyms:Carbonic acid adamantan-1-yl ester 4-[bis-(2-iodo-ethyl)-amino]-phenyl ester

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Chemical Property of Carbonic acid adamantan-1-yl ester 4-[bis-(2-iodo-ethyl)-amino]-phenyl ester

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Technology Process of Carbonic acid adamantan-1-yl ester 4-[bis-(2-iodo-ethyl)-amino]-phenyl ester

There total 4 articles about Carbonic acid adamantan-1-yl ester 4-[bis-(2-iodo-ethyl)-amino]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 172973-98-7
1-adamantyl 4-amino>phenyl carbonate

: 172973-93-2
Carbonic acid adamantan-1-yl ester 4-[bis-(2-iodo-ethyl)-amino]-phenyl ester

Guidance literature:: With sodium iodide; In acetonitrile; at 70 ℃;
DOI:10.1021/jm00026a013

Reference yield:

: 5854-73-9
1-Adamantyl-p-nitrophenyl-carbonat

: 172973-93-2
Carbonic acid adamantan-1-yl ester 4-[bis-(2-iodo-ethyl)-amino]-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium formate / 10percent Pd/C / ethanol

2: 82 percent / AcOH / 48 h / Ambient temperature

3: 48 percent / pyridine / a) 0 deg C, 40 min, b) 50 deg C, 18 min

4: 73 percent / NaI / acetonitrile / 70 °C

With pyridine; ammonium formate; acetic acid; sodium iodide; palladium on activated charcoal; In ethanol; acetonitrile;
DOI:10.1021/jm00026a013

Reference yield:

: 172974-25-3
Carbonic acid adamantan-1-yl ester 4-amino-phenyl ester

: 172973-93-2
Carbonic acid adamantan-1-yl ester 4-[bis-(2-iodo-ethyl)-amino]-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / AcOH / 48 h / Ambient temperature

2: 48 percent / pyridine / a) 0 deg C, 40 min, b) 50 deg C, 18 min

3: 73 percent / NaI / acetonitrile / 70 °C

With pyridine; acetic acid; sodium iodide; In acetonitrile;
DOI:10.1021/jm00026a013