Carbonic acid adamantan-1-yl ester 4-[bis-(2-hydroxy-ethyl)-amino]-phenyl ester

Base Information

• Chemical Name: Carbonic acid adamantan-1-yl ester 4-[bis-(2-hydroxy-ethyl)-amino]-phenyl ester
• CAS No.: 172973-90-9
• Molecular Formula: C₂₁H₂₉NO₅
• Molecular Weight: 375.465

Synonyms:Carbonic acid adamantan-1-yl ester 4-[bis-(2-hydroxy-ethyl)-amino]-phenyl ester

Chemical Property of Carbonic acid adamantan-1-yl ester 4-[bis-(2-hydroxy-ethyl)-amino]-phenyl ester

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Technology Process of Carbonic acid adamantan-1-yl ester 4-[bis-(2-hydroxy-ethyl)-amino]-phenyl ester

There total 2 articles about Carbonic acid adamantan-1-yl ester 4-[bis-(2-hydroxy-ethyl)-amino]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

oxirane (75-21-8,99932-75-9) + Carbonic acid adamantan-1-yl ester 4-amino-phenyl ester (172974-25-3) → Carbonic acid adamantan-1-yl ester 4-[bis-(2-hydroxy-ethyl)-amino]-phenyl ester (172973-90-9)

Guidance literature:

With acetic acid; for 48h; Ambient temperature;

DOI:10.1021/jm00026a013

Reference yield:

1-Adamantyl-p-nitrophenyl-carbonat (5854-73-9) → Carbonic acid adamantan-1-yl ester 4-[bis-(2-hydroxy-ethyl)-amino]-phenyl ester (172973-90-9)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium formate / 10percent Pd/C / ethanol

2: 82 percent / AcOH / 48 h / Ambient temperature

With ammonium formate; acetic acid; palladium on activated charcoal; In ethanol;

DOI:10.1021/jm00026a013

Reference yield: 48.0%

methanesulfonyl chloride (124-63-0) + Carbonic acid adamantan-1-yl ester 4-[bis-(2-hydroxy-ethyl)-amino]-phenyl ester (172973-90-9) → 1-adamantyl 4-phenyl carbonate + 1-adamantyl 4-<(2-chloroethyl)<2-(mesyloxy)ethyl>amino>phenyl carbonate (172973-94-3) + 1-adamantyl 4-amino>phenyl carbonate (172973-98-7)

Guidance literature:

With pyridine; a) 0 deg C, 40 min, b) 50 deg C, 18 min;

DOI:10.1021/jm00026a013

upstream raw materials:

oxirane

Carbonic acid adamantan-1-yl ester 4-amino-phenyl ester

1-Adamantyl-p-nitrophenyl-carbonat

Downstream raw materials:

1-adamantyl 4-<(2-chloroethyl)<2-(mesyloxy)ethyl>amino>phenyl carbonate

1-adamantyl 4-amino>phenyl carbonate

4-[bis-(2-bromo-ethyl)-amino]-phenol

Carbonic acid adamantan-1-yl ester 4-[bis-(2-bromo-ethyl)-amino]-phenyl ester

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