2-[2,6-dimethoxy-4-(methoxymethyl)phenyl]-5,5-dimethyl-1,3, 2-dioxaborinane

Base Information

Chemical Name:2-[2,6-dimethoxy-4-(methoxymethyl)phenyl]-5,5-dimethyl-1,3, 2-dioxaborinane
CAS No.:1144100-31-1
Molecular Formula:C₁₅H₂₃BO₅
Molecular Weight:294.156
Hs Code.:

Synonyms:2-[2,6-dimethoxy-4-(methoxymethyl)phenyl]-5,5-dimethyl-1,3, 2-dioxaborinane

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Chemical Property of 2-[2,6-dimethoxy-4-(methoxymethyl)phenyl]-5,5-dimethyl-1,3, 2-dioxaborinane

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Technology Process of 2-[2,6-dimethoxy-4-(methoxymethyl)phenyl]-5,5-dimethyl-1,3, 2-dioxaborinane

There total 1 articles about 2-[2,6-dimethoxy-4-(methoxymethyl)phenyl]-5,5-dimethyl-1,3, 2-dioxaborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.6%

: 685886-78-6
2-bromo-1,3-dimethoxy-5-(methoxymethyl)benzene

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 1144100-31-1
2-[2,6-dimethoxy-4-(methoxymethyl)phenyl]-5,5-dimethyl-1,3, 2-dioxaborinane

Guidance literature:: 2-bromo-1,3-dimethoxy-5-(methoxymethyl)benzene; With magnesium; iodine; In tetrahydrofuran; at 80 ℃;

With Triisopropyl borate; In tetrahydrofuran; at -0.4 - 20 ℃;

2,2-Dimethyl-1,3-propanediol; With acetic acid; In tetrahydrofuran; at 20 ℃; for 18.1h; Cooling with ice;

Reference yield:

: N-cyclopropylmethyl-N-(2-ethyl-7-iodopyrazolo[1,5-a]pyridine-3-yl)-N-(tetrahydro-2H-pyran-4-ylmethyl)amine

: 1144100-31-1
2-[2,6-dimethoxy-4-(methoxymethyl)phenyl]-5,5-dimethyl-1,3, 2-dioxaborinane

: 685885-75-0
N-(cyclopropylmethyl)-7-[2,6-dimethoxy-4-(methoxymethyl)phenyl]-2-ethyl-N-[(tetrahydro-2H-pyran-4-yl)methyl]pyrazolo[1,5-a]pyridin-3-amine

Guidance literature:: With potassium carbonate; palladium diacetate; triphenylphosphine; In 1,2-dimethoxyethane; water; at 90 ℃; for 14.6h; Product distribution / selectivity; Inert atmosphere;