3,4-dimethoxy-7-(2-oxo-6-phenylsulfonyl-5E-hexenyl)bicyclo<4.2.0>octa-1(6),2,4-triene-7-carbonitrile

Base Information

Chemical Name:3,4-dimethoxy-7-(2-oxo-6-phenylsulfonyl-5E-hexenyl)bicyclo<4.2.0>octa-1(6),2,4-triene-7-carbonitrile
CAS No.:96917-56-5
Molecular Formula:C₂₃H₂₃NO₅S
Molecular Weight:425.505
Hs Code.:

Synonyms:3,4-dimethoxy-7-(2-oxo-6-phenylsulfonyl-5E-hexenyl)bicyclo<4.2.0>octa-1(6),2,4-triene-7-carbonitrile

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Chemical Property of 3,4-dimethoxy-7-(2-oxo-6-phenylsulfonyl-5E-hexenyl)bicyclo<4.2.0>octa-1(6),2,4-triene-7-carbonitrile

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Technology Process of 3,4-dimethoxy-7-(2-oxo-6-phenylsulfonyl-5E-hexenyl)bicyclo<4.2.0>octa-1(6),2,4-triene-7-carbonitrile

There total 6 articles about 3,4-dimethoxy-7-(2-oxo-6-phenylsulfonyl-5E-hexenyl)bicyclo<4.2.0>octa-1(6),2,4-triene-7-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.3%

: 96917-55-4
3,4-dimethoxy-7-(2-oxo-6-phenylsulfinyl-6-phenylsulfonylhexyl)bicyclo<4.2.0>octa-1(6),2,4-triene-7-carbonitrile

: 96917-56-5
3,4-dimethoxy-7-(2-oxo-6-phenylsulfonyl-5E-hexenyl)bicyclo<4.2.0>octa-1(6),2,4-triene-7-carbonitrile

Guidance literature:: With sodium hydrogencarbonate; In toluene; for 0.5h; Heating;

Reference yield:

: 69543-15-3
1-bromomethylcyclopentene

: 96917-56-5
3,4-dimethoxy-7-(2-oxo-6-phenylsulfonyl-5E-hexenyl)bicyclo<4.2.0>octa-1(6),2,4-triene-7-carbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 74.4 percent / liquid ammonia, sodium amide / tetrahydrofuran / 2 h / -34 °C

2: osmium tetraoxide, sodium periodate

3: boron trifluoride etherate / CH₂Cl₂

4: 1.) m-chloroperbenzoic acid / 2.) thermally elimination

With sodium periodate; osmium(VIII) oxide; boron trifluoride diethyl etherate; ammonia; sodium amide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 35202-54-1
3,4-dimethoxy-bicyclo[4.2.0]octa-1,3,5-triene-7-carbonitrile

: 96917-56-5
3,4-dimethoxy-7-(2-oxo-6-phenylsulfonyl-5E-hexenyl)bicyclo<4.2.0>octa-1(6),2,4-triene-7-carbonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 74.4 percent / liquid ammonia, sodium amide / tetrahydrofuran / 2 h / -34 °C

2: osmium tetraoxide, sodium periodate

3: boron trifluoride etherate / CH₂Cl₂

4: 1.) m-chloroperbenzoic acid / 2.) thermally elimination

With sodium periodate; osmium(VIII) oxide; boron trifluoride diethyl etherate; ammonia; sodium amide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;