(4-Chloro-phenoxy)-acetic acid (1S,2S,3R,4S,5S,6S)-3,4,5-tris-[2-(4-chloro-phenoxy)-acetoxy]-2-[2,7-dibromo-9-(3-trifluoromethyl-phenyl)-9H-xanthen-9-yloxy]-6-(4-methoxy-tetrahydro-pyran-4-yloxy)-cyclohexyl ester

Base Information

Chemical Name:(4-Chloro-phenoxy)-acetic acid (1S,2S,3R,4S,5S,6S)-3,4,5-tris-[2-(4-chloro-phenoxy)-acetoxy]-2-[2,7-dibromo-9-(3-trifluoromethyl-phenyl)-9H-xanthen-9-yloxy]-6-(4-methoxy-tetrahydro-pyran-4-yloxy)-cyclohexyl ester
CAS No.:201860-72-2
Molecular Formula:C₆₄H₅₁Br₂Cl₄F₃O₁₇
Molecular Weight:1450.71
Hs Code.:

(4-Chloro-phenoxy)-acetic acid (1S,2S,3R,4S,5S,6S)-3,4,5-tris-[2-(4-chloro-phenoxy)-acetoxy]-2-[2,7-dibromo-9-(3-trifluoromethyl-phenyl)-9H-xanthen-9-yloxy]-6-(4-methoxy-tetrahydro-pyran-4-yloxy)-cyclohexyl ester

Synonyms:(4-Chloro-phenoxy)-acetic acid (1S,2S,3R,4S,5S,6S)-3,4,5-tris-[2-(4-chloro-phenoxy)-acetoxy]-2-[2,7-dibromo-9-(3-trifluoromethyl-phenyl)-9H-xanthen-9-yloxy]-6-(4-methoxy-tetrahydro-pyran-4-yloxy)-cyclohexyl ester

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Chemical Property of (4-Chloro-phenoxy)-acetic acid (1S,2S,3R,4S,5S,6S)-3,4,5-tris-[2-(4-chloro-phenoxy)-acetoxy]-2-[2,7-dibromo-9-(3-trifluoromethyl-phenyl)-9H-xanthen-9-yloxy]-6-(4-methoxy-tetrahydro-pyran-4-yloxy)-cyclohexyl ester

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Technology Process of (4-Chloro-phenoxy)-acetic acid (1S,2S,3R,4S,5S,6S)-3,4,5-tris-[2-(4-chloro-phenoxy)-acetoxy]-2-[2,7-dibromo-9-(3-trifluoromethyl-phenyl)-9H-xanthen-9-yloxy]-6-(4-methoxy-tetrahydro-pyran-4-yloxy)-cyclohexyl ester

There total 8 articles about (4-Chloro-phenoxy)-acetic acid (1S,2S,3R,4S,5S,6S)-3,4,5-tris-[2-(4-chloro-phenoxy)-acetoxy]-2-[2,7-dibromo-9-(3-trifluoromethyl-phenyl)-9H-xanthen-9-yloxy]-6-(4-methoxy-tetrahydro-pyran-4-yloxy)-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 4122-68-3
4-chlorophenyloxyacetyl chloride

: 201860-70-0
6-O-{2,7-Dibromo-9-[3-(trifluoromethyl)phenyl]xanthen-9-yl}-2-O-(4-methoxytetrahydropyran-4-yl)-D-myo-inositol

: 201860-71-1
3,4,5-Tris-O-[(4-chlorophenoxy)acetyl]-6-O-{2,7-dibromo-9-[3-(trifluoromethyl)phenyl]xanthen-9-yl}-2-O-(4-methoxytetrahydropyran-4-yl)-D-myo-inositol

: 201860-72-2
(4-Chloro-phenoxy)-acetic acid (1S,2S,3R,4S,5S,6S)-3,4,5-tris-[2-(4-chloro-phenoxy)-acetoxy]-2-[2,7-dibromo-9-(3-trifluoromethyl-phenyl)-9H-xanthen-9-yloxy]-6-(4-methoxy-tetrahydro-pyran-4-yloxy)-cyclohexyl ester

Guidance literature:: With pyridine; dmap; 3-nitro-1,2,4-triazole; In acetonitrile; Ambient temperature;
DOI:10.1016/S0960-894X(97)10166-4

Reference yield:

: 17327-22-9
4-methoxy-2,6-dihydropyran

: 201860-72-2
(4-Chloro-phenoxy)-acetic acid (1S,2S,3R,4S,5S,6S)-3,4,5-tris-[2-(4-chloro-phenoxy)-acetoxy]-2-[2,7-dibromo-9-(3-trifluoromethyl-phenyl)-9H-xanthen-9-yloxy]-6-(4-methoxy-tetrahydro-pyran-4-yloxy)-cyclohexyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 44.73 g / Ph₃P*HBr / CH₂Cl₂ / 40 h / 20 °C

2: 18.27 g / NaOMe / methanol; tetrahydrofuran / 0.5 h / 20 °C

3: 62.8 percent / imidazole; Et₃N / hexamethylphosphoric acid triamide / 60 h / 20 °C

4: 73 percent / pyridine / acetonitrile / 1.33 h / 20 °C

5: 4.33 g / Et₄NF / acetonitrile / 0.5 h / 20 °C

6: 1H-tetrazole; pyridine; DMAP / acetonitrile / 1.58 h / 20 °C

With pyridine; 1H-imidazole; 1H-tetrazole; dmap; sodium methylate; triphenylphosphine hydrobromide; tetraethylammonium fluoride; triethylamine; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; acetonitrile;
DOI:10.1039/b007267m

Reference yield:

: 201860-64-2
2-O-(4-Methoxytetrahydropyran-4-yl)-myo-inositol

: 201860-72-2
(4-Chloro-phenoxy)-acetic acid (1S,2S,3R,4S,5S,6S)-3,4,5-tris-[2-(4-chloro-phenoxy)-acetoxy]-2-[2,7-dibromo-9-(3-trifluoromethyl-phenyl)-9H-xanthen-9-yloxy]-6-(4-methoxy-tetrahydro-pyran-4-yloxy)-cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 62.8 percent / imidazole; Et₃N / hexamethylphosphoric acid triamide / 60 h / 20 °C

2: 73 percent / pyridine / acetonitrile / 1.33 h / 20 °C

3: 4.33 g / Et₄NF / acetonitrile / 0.5 h / 20 °C

4: 1H-tetrazole; pyridine; DMAP / acetonitrile / 1.58 h / 20 °C

With pyridine; 1H-imidazole; 1H-tetrazole; dmap; tetraethylammonium fluoride; triethylamine; In N,N,N,N,N,N-hexamethylphosphoric triamide; acetonitrile;
DOI:10.1039/b007267m