(C₆H₃(CH₂CH₃)CH(CH₃)2)2NC(CH₃)CHC(CH₃)NZnCH₂CH₃

Base Information

• Chemical Name: (C₆H₃(CH₂CH₃)CH(CH₃)2)2NC(CH₃)CHC(CH₃)NZnCH₂CH₃
• CAS No.: 369404-51-3
• Molecular Formula: C₂₉H₄₂N₂Zn
• Molecular Weight: 484.056
• Mol file: 369404-51-3.mol

Synonyms:(C₆H₃(CH₂CH₃)CH(CH₃)2)2NC(CH₃)CHC(CH₃)NZnCH₂CH₃

Chemical Property of (C₆H₃(CH₂CH₃)CH(CH₃)2)2NC(CH₃)CHC(CH₃)NZnCH₂CH₃

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (C₆H₃(CH₂CH₃)CH(CH₃)2)2NC(CH₃)CHC(CH₃)NZnCH₂CH₃

There total 1 articles about (C₆H₃(CH₂CH₃)CH(CH₃)2)2NC(CH₃)CHC(CH₃)NZnCH₂CH₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(C6H3(CH2CH3)(CH(CH3)2))2NC(CH3)CHC(CH3)NH + diethylzinc (557-20-0) → (C6H3(CH2CH3)CH(CH3)2)2NC(CH3)CHC(CH3)NZnCH2CH3 (369404-51-3)

Guidance literature:

In toluene; (N2); addn. of a soln. of ligand in toluene to a soln. of ZnEt2 in toluene at 0°C, stirring overnight at 80°C; drying in vac.;

DOI:10.1021/ja003850n

Reference yield: 38.0%

methanol (67-56-1) + (C6H3(CH2CH3)CH(CH3)2)2NC(CH3)CHC(CH3)NZnCH2CH3 (369404-51-3) → [(C6H3(CH(CH3)2)CH2CH3)2NC(CH3)CHC(CH3)NZn(OCH3)]2 (369404-58-0)

Guidance literature:

In toluene; (N2); addn. of methanol to a soln. of zinc complex in toluene at room temp., stirring for 1 h at room temp.; filtration, drying in vac., recrystn. (toluene, -30°C);

DOI:10.1021/ja003850n

upstream raw materials:

diethylzinc

Downstream raw materials:

[(C₆H₃(CH(CH₃)2)CH₂CH₃)2NC(CH₃)CHC(CH₃)NZn(OCH₃)]2