C₁₅H₁₉NO

Base Information

Chemical Name:C₁₅H₁₉NO
CAS No.:1407547-48-1
Molecular Formula:C₁₅H₁₉NO
Molecular Weight:229.322
Hs Code.:

Synonyms:C₁₅H₁₉NO

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Chemical Property of C₁₅H₁₉NO

Chemical Property:

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Technology Process of C₁₅H₁₉NO

There total 4 articles about C₁₅H₁₉NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1407547-45-8
(3S,3aR,8aS)-3-phenyl-1-[(1R)-1-phenylethyl]octahydrocyclohepta[b]pyrrol-4(1H)-one

: 1407547-48-1
C₁₅H₁₉NO

Guidance literature:: With hydrogenchloride; 5%-palladium/activated carbon; hydrogen; In ethanol; under 760.051 Torr; stereoselective reaction;
DOI:10.1021/jo301762a

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1407547-48-1
C₁₅H₁₉NO

Guidance literature:: Multi-step reaction with 7 steps

1: n-butyllithium; cerium(III) chloride / tetrahydrofuran / -78 °C

2: triethylamine; methanesulfonyl chloride / dichloromethane / -20 °C

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C

4: lithium perchlorate / acetonitrile / 65 °C

5: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether / 2 h / 0 - 20 °C

6: camphor-10-sulfonic acid; sodium sulfate / water; dichloromethane / 20 °C

7: 5%-palladium/activated carbon; hydrogenchloride; hydrogen / ethanol / 760.05 Torr

With hydrogenchloride; n-butyllithium; cerium(III) chloride; 5%-palladium/activated carbon; camphor-10-sulfonic acid; hydrogen; lithium perchlorate; methanesulfonyl chloride; sodium sulfate; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; acetonitrile; 6: |Mannich Aminomethylation;
DOI:10.1021/jo301762a

Reference yield:

: 20109-09-5
1-(phenylethynyl)-1-cyclohexanol

: 1407547-48-1
C₁₅H₁₉NO

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine; methanesulfonyl chloride / dichloromethane / -20 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 °C

3: lithium perchlorate / acetonitrile / 65 °C

4: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether / 2 h / 0 - 20 °C

5: camphor-10-sulfonic acid; sodium sulfate / water; dichloromethane / 20 °C

6: 5%-palladium/activated carbon; hydrogenchloride; hydrogen / ethanol / 760.05 Torr

With hydrogenchloride; 5%-palladium/activated carbon; camphor-10-sulfonic acid; hydrogen; lithium perchlorate; methanesulfonyl chloride; sodium sulfate; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium bis(2-methoxyethoxy)aluminium dihydride; In diethyl ether; ethanol; dichloromethane; water; acetonitrile; 5: |Mannich Aminomethylation;
DOI:10.1021/jo301762a