C₂₂H₂₈FNO₃S

Base Information

Chemical Name:C₂₂H₂₈FNO₃S
CAS No.:1193512-80-9
Molecular Formula:C₂₂H₂₈FNO₃S
Molecular Weight:405.534
Hs Code.:

C<sub>22</sub>H<sub>28</sub>FNO<sub>3</sub>S

Synonyms:C₂₂H₂₈FNO₃S

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Chemical Property of C₂₂H₂₈FNO₃S

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Technology Process of C₂₂H₂₈FNO₃S

There total 15 articles about C₂₂H₂₈FNO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1193512-78-5
C₂₂H₂₆FNO₅S

: 1193512-80-9
C₂₂H₂₈FNO₃S

Guidance literature:: With hydrogen; 5%-palladium/activated carbon; In ethanol; dichloromethane; under 2250.23 Torr;

Reference yield:

: 540-36-3
para-difluorobenzene

: 1193512-80-9
C₂₂H₂₈FNO₃S

Guidance literature:: Multi-step reaction with 7 steps

1.1: aluminum (III) chloride / 16 h / 20 °C / Reflux

2.1: potassium carbonate; tetrabutylammomium bromide / toluene / 24 h / Reflux

2.2: 12 h

2.3: 1.5 h

3.1: boron trifluoride diethyl etherate; triethylsilane / 8 h / 65 °C

4.1: potassium carbonate / acetonitrile; ethanol; water / 5 °C

4.2: 1 h

5.1: sodium hydrogencarbonate; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; sodium hypochlorite; sodium bromide / dichloromethane; water / 2 h

6.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

7.1: hydrogen / 5%-palladium/activated carbon / dichloromethane; ethanol / 2250.23 Torr

With triethylsilane; aluminum (III) chloride; sodium hypochlorite; boron trifluoride diethyl etherate; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; potassium tert-butylate; tetrabutylammomium bromide; hydrogen; sodium hydrogencarbonate; potassium carbonate; sodium bromide; 5%-palladium/activated carbon; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; acetonitrile;

Reference yield:

: 121-90-4
m-nitrobenzoic acid chloride

: 1193512-80-9
C₂₂H₂₈FNO₃S

Guidance literature:: Multi-step reaction with 7 steps

1.1: aluminum (III) chloride / 16 h / 20 °C / Reflux

2.1: potassium carbonate; tetrabutylammomium bromide / toluene / 24 h / Reflux

2.2: 12 h

2.3: 1.5 h

3.1: boron trifluoride diethyl etherate; triethylsilane / 8 h / 65 °C

4.1: potassium carbonate / acetonitrile; ethanol; water / 5 °C

4.2: 1 h

5.1: sodium hydrogencarbonate; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; sodium hypochlorite; sodium bromide / dichloromethane; water / 2 h

6.1: potassium tert-butylate / tetrahydrofuran / 1 h / 0 °C

7.1: hydrogen / 5%-palladium/activated carbon / dichloromethane; ethanol / 2250.23 Torr

With triethylsilane; aluminum (III) chloride; sodium hypochlorite; boron trifluoride diethyl etherate; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; potassium tert-butylate; tetrabutylammomium bromide; hydrogen; sodium hydrogencarbonate; potassium carbonate; sodium bromide; 5%-palladium/activated carbon; In tetrahydrofuran; ethanol; dichloromethane; water; toluene; acetonitrile;