(8-chloro-2-phenyl-4H-5-oxa-3,9b-diaza-cyclopenta[a]naphthalen-4-yl)-acetic acid methyl ester

Base Information

Chemical Name:(8-chloro-2-phenyl-4H-5-oxa-3,9b-diaza-cyclopenta[a]naphthalen-4-yl)-acetic acid methyl ester
CAS No.:915725-01-8
Molecular Formula:C₁₉H₁₅ClN₂O₃
Molecular Weight:354.793
Hs Code.:

(8-chloro-2-phenyl-4<i>H</i>-5-oxa-3,9b-diaza-cyclopenta[<i>a</i>]naphthalen-4-yl)-acetic acid methyl ester

Synonyms:(8-chloro-2-phenyl-4H-5-oxa-3,9b-diaza-cyclopenta[a]naphthalen-4-yl)-acetic acid methyl ester

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Chemical Property of (8-chloro-2-phenyl-4H-5-oxa-3,9b-diaza-cyclopenta[a]naphthalen-4-yl)-acetic acid methyl ester

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Technology Process of (8-chloro-2-phenyl-4H-5-oxa-3,9b-diaza-cyclopenta[a]naphthalen-4-yl)-acetic acid methyl ester

There total 3 articles about (8-chloro-2-phenyl-4H-5-oxa-3,9b-diaza-cyclopenta[a]naphthalen-4-yl)-acetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 915724-91-3
[6-chloro-3-oxo-4-(2-oxo-2-phenyl-ethyl)-3,4-dihydro-2H-benzo[1,4]oxazin-2-yl]-acetic acid methyl ester

: 915725-01-8
(8-chloro-2-phenyl-4H-5-oxa-3,9b-diaza-cyclopenta[a]naphthalen-4-yl)-acetic acid methyl ester

Guidance literature:: With ammonium acetate; acetic acid; for 4h; Heating;

Reference yield:

: 104662-84-2
(6-Chloro-3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-2-yl)-acetic acid methyl ester

: 915725-01-8
(8-chloro-2-phenyl-4H-5-oxa-3,9b-diaza-cyclopenta[a]naphthalen-4-yl)-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / anhydrous potassium carbonate; tetrabutylammonium bromide / acetone / Heating

2: 72 percent / ammonium acetate; glacial acetic acid / 4 h / Heating

With ammonium acetate; tetrabutylammomium bromide; potassium carbonate; acetic acid; In acetone;

Reference yield:

: 70-11-1
α-bromoacetophenone

: 915725-01-8
(8-chloro-2-phenyl-4H-5-oxa-3,9b-diaza-cyclopenta[a]naphthalen-4-yl)-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / anhydrous potassium carbonate; tetrabutylammonium bromide / acetone / Heating

2: 72 percent / ammonium acetate; glacial acetic acid / 4 h / Heating

With ammonium acetate; tetrabutylammomium bromide; potassium carbonate; acetic acid; In acetone;