N,N-bis(tert-butoxycarbonyl)-O-(tert-butoxycarbonyl)-L-tyrosine methyl ester

Base Information

Chemical Name:N,N-bis(tert-butoxycarbonyl)-O-(tert-butoxycarbonyl)-L-tyrosine methyl ester
CAS No.:911663-30-4
Molecular Formula:C₂₅H₃₇NO₉
Molecular Weight:495.57
Hs Code.:

Synonyms:N,N-bis(tert-butoxycarbonyl)-O-(tert-butoxycarbonyl)-L-tyrosine methyl ester

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Chemical Property of N,N-bis(tert-butoxycarbonyl)-O-(tert-butoxycarbonyl)-L-tyrosine methyl ester

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Technology Process of N,N-bis(tert-butoxycarbonyl)-O-(tert-butoxycarbonyl)-L-tyrosine methyl ester

There total 2 articles about N,N-bis(tert-butoxycarbonyl)-O-(tert-butoxycarbonyl)-L-tyrosine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 3417-91-2
L-tyrosine methyl ester HCl

: 911663-30-4
N,N-bis(tert-butoxycarbonyl)-O-(tert-butoxycarbonyl)-L-tyrosine methyl ester

Guidance literature:: L-tyrosine methyl ester HCl; With sodium carbonate; In tetrahydrofuran; water; at 20 ℃; for 2h;

di-tert-butyl dicarbonate; With dmap; In acetonitrile; at 20 ℃; for 12h;
DOI:10.1021/jo061159i

Reference yield: 100.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1080-06-4
L-Tyr-OMe

: 911663-30-4
N,N-bis(tert-butoxycarbonyl)-O-(tert-butoxycarbonyl)-L-tyrosine methyl ester

Guidance literature:: With dmap;
DOI:10.1021/jo061159i

Reference yield: 65.0%

: 911663-30-4
N,N-bis(tert-butoxycarbonyl)-O-(tert-butoxycarbonyl)-L-tyrosine methyl ester

: 911663-34-8
3-(tert-butyl) 4-methyl (4S,5R)-5-(4-((tert-butoxycarbonyl)oxy)phenyl)-2-oxazolidin-2-one-3,4-dicarboxylate

Guidance literature:: N,N-bis(tert-butoxycarbonyl)-O-(tert-butoxycarbonyl)-L-tyrosine methyl ester; With N-Bromosuccinimide; In tetrachloromethane; for 1.5h; Reflux; Inert atmosphere; Irradiation;

With silver nitrate; In acetone; at 20 ℃; for 4h;
DOI:10.1021/acs.orglett.0c02884