C₂₇H₄₁ClO₂

Base Information

Chemical Name:C₂₇H₄₁ClO₂
CAS No.:1579830-33-3
Molecular Formula:C₂₇H₄₁ClO₂
Molecular Weight:433.074
Hs Code.:

C<sub>27</sub>H<sub>41</sub>ClO<sub>2</sub>

Synonyms:C₂₇H₄₁ClO₂

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Chemical Property of C₂₇H₄₁ClO₂

Chemical Property:

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Technology Process of C₂₇H₄₁ClO₂

There total 1 articles about C₂₇H₄₁ClO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14773-00-3
methyl (5β,7α)-12-hydroxy-3-oxo-cholan-24-oate

: 1579830-33-3
C₂₇H₄₁ClO₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / 20 °C

1.2: 0 °C

2.1: 2-iodoxybenzoic acid; trifluoroacetic acid / dimethyl sulfoxide / 60 °C / Darkness

3.1: lithium; ammonia / tert-butyl alcohol; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine; lithium chloride / acetonitrile / 0.25 h / 20 °C

4.2: 20 °C

5.1: Burgess Reagent / toluene / Reflux

6.1: lithium hydroxide / methanol; tetrahydrofuran; water / 20 °C

7.1: methanol / 0.25 h / Inert atmosphere

7.2: 3.02 h / 50 °C

8.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 0.33 h / Inert atmosphere

With oxalyl dichloride; Burgess Reagent; 2-iodoxybenzoic acid; ammonia; lithium; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium chloride; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol; 5.1: |Burgess Alcohol Dehydration;
DOI:10.1002/anie.201307465