2,2-dichloro-1-phenylcyclopropanecarbaldehyde diethyl acetal

Base Information

Chemical Name:2,2-dichloro-1-phenylcyclopropanecarbaldehyde diethyl acetal
CAS No.:156020-80-3
Molecular Formula:C₁₄H₁₈Cl₂O₂
Molecular Weight:289.202
Hs Code.:

Synonyms:2,2-dichloro-1-phenylcyclopropanecarbaldehyde diethyl acetal

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Chemical Property of 2,2-dichloro-1-phenylcyclopropanecarbaldehyde diethyl acetal

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Technology Process of 2,2-dichloro-1-phenylcyclopropanecarbaldehyde diethyl acetal

There total 1 articles about 2,2-dichloro-1-phenylcyclopropanecarbaldehyde diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 67-66-3,8013-54-5
chloroform

: 80234-04-4
2-phenylacrylaldehyde diethyl acetal

: 156020-80-3
2,2-dichloro-1-phenylcyclopropanecarbaldehyde diethyl acetal

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; water; at 40 ℃; for 2h;
DOI:10.1039/P19940000739

Reference yield: 74.0%

: 156020-80-3
2,2-dichloro-1-phenylcyclopropanecarbaldehyde diethyl acetal

: 122801-51-8
2,2-dichloro-1-phenylcyclopropane-1-carbaldehyde

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 60 ℃; for 8h;
DOI:10.1039/P19940000739

Reference yield:

: 156020-80-3
2,2-dichloro-1-phenylcyclopropanecarbaldehyde diethyl acetal

: 122801-37-0
4-chloro-2,5-diphenylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / conc. HCl / tetrahydrofuran; H₂O / 8 h / 60 °C

2: Na₂SO₄ / benzene / 12 h / Ambient temperature

3: 2 percent / benzene / 200 °C

With hydrogenchloride; sodium sulfate; In tetrahydrofuran; water; benzene;
DOI:10.1039/P19940000739