1-(3-benzyloxy-4-methoxybenzyl)-8-methoxy-6,7-methylenedioxyisoquinoline

Base Information

Chemical Name:1-(3-benzyloxy-4-methoxybenzyl)-8-methoxy-6,7-methylenedioxyisoquinoline
CAS No.:79667-52-0
Molecular Formula:C₂₆H₂₃NO₅
Molecular Weight:429.472
Hs Code.:

Synonyms:1-(3-benzyloxy-4-methoxybenzyl)-8-methoxy-6,7-methylenedioxyisoquinoline

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Chemical Property of 1-(3-benzyloxy-4-methoxybenzyl)-8-methoxy-6,7-methylenedioxyisoquinoline

Chemical Property:

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Technology Process of 1-(3-benzyloxy-4-methoxybenzyl)-8-methoxy-6,7-methylenedioxyisoquinoline

There total 4 articles about 1-(3-benzyloxy-4-methoxybenzyl)-8-methoxy-6,7-methylenedioxyisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 82958-03-0
6-Benzoyl-5-(3-benzyloxy-4-methoxy-benzyl)-4-methoxy-5,6-dihydro-[1,3]dioxolo[4,5-g]isoquinoline-5-carbonitrile

: 79667-52-0
1-(3-benzyloxy-4-methoxybenzyl)-8-methoxy-6,7-methylenedioxyisoquinoline

Guidance literature:: With sodium hydroxide; In ethanol; water; for 2.5h; Heating;

Reference yield:

: 5361-66-0
8-methoxy-6,7-methylenedioxyisoquinoline

: 79667-52-0
1-(3-benzyloxy-4-methoxybenzyl)-8-methoxy-6,7-methylenedioxyisoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / CH₂Cl₂; H₂O / 1 h / Ambient temperature

2: NaH / dimethylformamide / 1.) -20 deg C, 2 h; 2.) room temperature, 3 h

3: 58 percent / sodium hydroxide / ethanol; H₂O / 2.5 h / Heating

With sodium hydroxide; sodium hydride; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1699-38-3
3-benzyloxy-4-methoxy-benzyl chloride

: 79667-52-0
1-(3-benzyloxy-4-methoxybenzyl)-8-methoxy-6,7-methylenedioxyisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: NaH / dimethylformamide / 1.) -20 deg C, 2 h; 2.) room temperature, 3 h

2: 58 percent / sodium hydroxide / ethanol; H₂O / 2.5 h / Heating

With sodium hydroxide; sodium hydride; In ethanol; water; N,N-dimethyl-formamide;