(-)-(1R,2S,3S,4S)-2,3-O-Allylborylen-2-endo-methyl-3-endo-phenyl-2-exo,3-exo-bornandiol

Base Information

Chemical Name:(-)-(1R,2S,3S,4S)-2,3-O-Allylborylen-2-endo-methyl-3-endo-phenyl-2-exo,3-exo-bornandiol
CAS No.:77078-92-3
Molecular Formula:C₂₀H₂₇BO₂
Molecular Weight:310.244
Hs Code.:

Synonyms:(-)-(1R,2S,3S,4S)-2,3-O-Allylborylen-2-endo-methyl-3-endo-phenyl-2-exo,3-exo-bornandiol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(1R,2S,3S,4S)-2,3-O-Allylborylen-2-endo-methyl-3-endo-phenyl-2-exo,3-exo-bornandiol

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Technology Process of (-)-(1R,2S,3S,4S)-2,3-O-Allylborylen-2-endo-methyl-3-endo-phenyl-2-exo,3-exo-bornandiol

There total 1 articles about (-)-(1R,2S,3S,4S)-2,3-O-Allylborylen-2-endo-methyl-3-endo-phenyl-2-exo,3-exo-bornandiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 688-61-9,53588-88-8,90721-85-0,151452-33-4,151452-35-6
Triallylborane

: 68303-63-9
(1R,2S,3S,4S)-2-endo-Methyl-3-endo-phenyl-2-exo,3-exo-bornandiol

: 77078-92-3
(-)-(1R,2S,3S,4S)-2,3-O-Allylborylen-2-endo-methyl-3-endo-phenyl-2-exo,3-exo-bornandiol

Guidance literature:: In tetrahydrofuran; byproducts: propene; B(C3H5)3 was added to a THF soln. of organic compd. at 25°C, mixture was refluxed for 1 h; THF was removed, residue was chromd.; elem. anal.;

Reference yield:

: 75-07-0,9002-91-9
acetaldehyde

: 77078-92-3
(-)-(1R,2S,3S,4S)-2,3-O-Allylborylen-2-endo-methyl-3-endo-phenyl-2-exo,3-exo-bornandiol

: 64584-92-5
(R)-pent-4-en-2-ol

: 625-31-0,64584-92-5,111957-98-3,55563-79-6
(S)-4-penten-2-ol

Guidance literature:: With triethanolamine; Multistep reaction. Title compound not separated from byproducts; 1.) propane, -90 deg C, 2 h; 12 h, 20 deg C, 2.) 2 h;