4-phenyl-1-(p-tolylsulfonyl)-3-[4-(2-pyrrolidin-1-ylethoxymethyl)-1-piperidyl]thieno[2,3-c]pyrazole

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Chemical Name:4-phenyl-1-(p-tolylsulfonyl)-3-[4-(2-pyrrolidin-1-ylethoxymethyl)-1-piperidyl]thieno[2,3-c]pyrazole
CAS No.:1436613-47-6
Molecular Formula:C₃₀H₃₆N₄O₃S₂
Molecular Weight:564.773
Hs Code.:

Synonyms:4-phenyl-1-(p-tolylsulfonyl)-3-[4-(2-pyrrolidin-1-ylethoxymethyl)-1-piperidyl]thieno[2,3-c]pyrazole

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Chemical Property of 4-phenyl-1-(p-tolylsulfonyl)-3-[4-(2-pyrrolidin-1-ylethoxymethyl)-1-piperidyl]thieno[2,3-c]pyrazole

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Technology Process of 4-phenyl-1-(p-tolylsulfonyl)-3-[4-(2-pyrrolidin-1-ylethoxymethyl)-1-piperidyl]thieno[2,3-c]pyrazole

There total 11 articles about 4-phenyl-1-(p-tolylsulfonyl)-3-[4-(2-pyrrolidin-1-ylethoxymethyl)-1-piperidyl]thieno[2,3-c]pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1436613-26-1
N-[(Z)-[(2,5-dibromo-4-phenyl-3-thienyl)-[4-(2-pyrrolidin-1-ylethoxymethyl)-1-piperidyl]methylene]amino]-4-methyl-benzenesulfonamide

: 1436613-47-6
4-phenyl-1-(p-tolylsulfonyl)-3-[4-(2-pyrrolidin-1-ylethoxymethyl)-1-piperidyl]thieno[2,3-c]pyrazole

Guidance literature:: With copper(l) iodide; potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 180 ℃; for 1h; Microwave irradiation;

Reference yield:

: 1248509-76-3
4-(2-pyrrolidin-1-ylethoxymethyl)piperidine

: 1436613-47-6
4-phenyl-1-(p-tolylsulfonyl)-3-[4-(2-pyrrolidin-1-ylethoxymethyl)-1-piperidyl]thieno[2,3-c]pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1,4-diaza-bicyclo[2.2.2]octane / tetrahydrofuran / 20 °C

2: copper(l) iodide; potassium carbonate / 1-methyl-pyrrolidin-2-one / 1 h / 180 °C / Microwave irradiation

With 1,4-diaza-bicyclo[2.2.2]octane; copper(l) iodide; potassium carbonate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one;

Reference yield:

: 1436612-96-2
2,5-dibromo-4-phenyl-thiophene-3-carboxylic acid

: 1436613-47-6
4-phenyl-1-(p-tolylsulfonyl)-3-[4-(2-pyrrolidin-1-ylethoxymethyl)-1-piperidyl]thieno[2,3-c]pyrazole

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride; N,N-dimethyl-formamide / dichloromethane / 2 h / Reflux

2: toluene / 2 h / 100 °C

3: thionyl chloride / 1 h / 80 °C

4: 1,4-diaza-bicyclo[2.2.2]octane / tetrahydrofuran / 20 °C

5: copper(l) iodide; potassium carbonate / 1-methyl-pyrrolidin-2-one / 1 h / 180 °C / Microwave irradiation

With 1,4-diaza-bicyclo[2.2.2]octane; copper(l) iodide; thionyl chloride; potassium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; toluene;