Technology Process of C32H6F10O4S4
There total 9 articles about C32H6F10O4S4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2,7-bis-(5-pentafluorobenzoyl-thiophene-2-yl)-benzo[1,2-b:6,5-b']dithiophene-4,5-bis(ethyleneoxolane);
With
acetic acid;
Reflux;
With
hydrogenchloride;
In
water;
for 2h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / toluene / Reflux
2.1: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 153 °C / Inert atmosphere
3.1: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / Inert atmosphere; Cooling with acetone-dry ice
3.2: 1 h
4.1: acetic acid / Reflux
4.2: 2 h / Reflux
With
tetrakis(triphenylphosphine) palladium(0); n-butyllithium; toluene-4-sulfonic acid; acetic acid;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: bromine / dichloromethane / Cooling with liquid nitrogen
2.1: toluene-4-sulfonic acid / toluene / Reflux
3.1: tetrakis(triphenylphosphine) palladium(0) / N,N-dimethyl-formamide / 153 °C / Inert atmosphere
4.1: n-butyllithium / tetrahydrofuran; hexane / 0.42 h / Inert atmosphere; Cooling with acetone-dry ice
4.2: 1 h
5.1: acetic acid / Reflux
5.2: 2 h / Reflux
With
tetrakis(triphenylphosphine) palladium(0); n-butyllithium; bromine; toluene-4-sulfonic acid; acetic acid;
In
tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; toluene;