Technology Process of 2-(1-cyclohexene-1-yl)ethanethiol acetate
There total 3 articles about 2-(1-cyclohexene-1-yl)ethanethiol acetate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 80 percent / LiAlH4 / diethyl ether / 1.5 h
2: 72.3 percent / pyridine / 26 h / 0 °C
3: 85.5 percent / tetrahydrofuran / 2 h / Heating
With
pyridine; lithium aluminium tetrahydride;
In
tetrahydrofuran; diethyl ether;
DOI:10.1139/v85-216
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 72.3 percent / pyridine / 26 h / 0 °C
2: 85.5 percent / tetrahydrofuran / 2 h / Heating
With
pyridine;
In
tetrahydrofuran;
DOI:10.1139/v85-216
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 85 percent / NaOH / H2O / 20 h / Heating
2: 80 percent / LiAlH4 / diethyl ether / 1.5 h
3: 72.3 percent / pyridine / 26 h / 0 °C
4: 85.5 percent / tetrahydrofuran / 2 h / Heating
With
pyridine; sodium hydroxide; lithium aluminium tetrahydride;
In
tetrahydrofuran; diethyl ether; water;
DOI:10.1139/v85-216
