[1-(2-phenylethyl)-1H-dibenzo[2,3:6,7]oxepino[4,5-d]imidazol-2-yl]methanol

Base Information

• Chemical Name: [1-(2-phenylethyl)-1H-dibenzo[2,3:6,7]oxepino[4,5-d]imidazol-2-yl]methanol
• CAS No.: 629620-76-4
• Molecular Formula: C₂₄H₂₀N₂O₂
• Molecular Weight: 368.435

Synonyms:[1-(2-phenylethyl)-1H-dibenzo[2,3:6,7]oxepino[4,5-d]imidazol-2-yl]methanol

Chemical Property of [1-(2-phenylethyl)-1H-dibenzo[2,3:6,7]oxepino[4,5-d]imidazol-2-yl]methanol

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Technology Process of [1-(2-phenylethyl)-1H-dibenzo[2,3:6,7]oxepino[4,5-d]imidazol-2-yl]methanol

There total 1 articles about [1-(2-phenylethyl)-1H-dibenzo[2,3:6,7]oxepino[4,5-d]imidazol-2-yl]methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

1-(2-phenylethyl)-1H-dibenzo[2,3:6,7]oxepino[4,5-d]imidazole-2-carbaldehyde → [1-(2-phenylethyl)-1H-dibenzo[2,3:6,7]oxepino[4,5-d]imidazol-2-yl]methanol (629620-76-4)

Guidance literature:

With sodium tetrahydroborate; In methanol; dichloromethane; at 20 ℃; for 2h;

DOI:10.1002/jhet.376

Reference yield: 72.0%

[1-(2-phenylethyl)-1H-dibenzo[2,3:6,7]oxepino[4,5-d]imidazol-2-yl]methanol (629620-76-4) + (2-chloroethyl)dimethylamine hydrochloride (4584-46-7) → dimethyl[2-({[1-(2-phenylethyl)-1H-dibenzo[2,3:6,7]oxepino[4,5-d]imidazol-2-yl]methyl}oxy)ethyl]amine (629620-89-9)

Guidance literature:

With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide; In water; toluene; at 109 ℃;

DOI:10.1002/jhet.376

Reference yield: 52.0%

[1-(2-phenylethyl)-1H-dibenzo[2,3:6,7]oxepino[4,5-d]imidazol-2-yl]methanol (629620-76-4) + 3-(dimethylamino)propyl chloride hydrochloride (5407-04-5) → dimethyl[3-({[1-(2-phenylethyl)-1H-dibenzo[2,3:6,7]oxepino[4,5-d]imidazol-2-yl]methyl}oxy)propyl]amine (629620-90-2)

Guidance literature:

With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide; In water; toluene; at 109 ℃;

DOI:10.1002/jhet.376

Downstream raw materials:

dimethyl[2-({[1-(2-phenylethyl)-1H-dibenzo[2,3:6,7]oxepino[4,5-d]imidazol-2-yl]methyl}oxy)ethyl]amine

dimethyl[3-({[1-(2-phenylethyl)-1H-dibenzo[2,3:6,7]oxepino[4,5-d]imidazol-2-yl]methyl}oxy)propyl]amine

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