2-[(4-Chloro-phenyl)-hydrazono]-3-oxo-3-phenyl-propionimidic acid ethyl ester

Base Information

Chemical Name:2-[(4-Chloro-phenyl)-hydrazono]-3-oxo-3-phenyl-propionimidic acid ethyl ester
CAS No.:126355-31-5
Molecular Formula:C₁₇H₁₆ClN₃O₂
Molecular Weight:329.786
Hs Code.:

Synonyms:2-[(4-Chloro-phenyl)-hydrazono]-3-oxo-3-phenyl-propionimidic acid ethyl ester

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Chemical Property of 2-[(4-Chloro-phenyl)-hydrazono]-3-oxo-3-phenyl-propionimidic acid ethyl ester

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Technology Process of 2-[(4-Chloro-phenyl)-hydrazono]-3-oxo-3-phenyl-propionimidic acid ethyl ester

There total 2 articles about 2-[(4-Chloro-phenyl)-hydrazono]-3-oxo-3-phenyl-propionimidic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2028-74-2
p-chlorobenzenediazonium chloride

: 91132-63-7
(E)-3-Amino-3-ethoxy-1-phenyl-2-propen-1-on

: 126355-31-5
2-[(4-Chloro-phenyl)-hydrazono]-3-oxo-3-phenyl-propionimidic acid ethyl ester

Guidance literature:: With sodium acetate; In ethanol; at 0 ℃; for 2h;
DOI:10.1055/s-1989-27393

Reference yield:

: 614-16-4
Benzoylacetonitrile

: 126355-31-5
2-[(4-Chloro-phenyl)-hydrazono]-3-oxo-3-phenyl-propionimidic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 1.) HCl, 2.) Et₃N / 1.) Et₂₀, 0 degC, 6 h, 2.) water, 15 min

2: 80 percent / NaOAc / ethanol / 2 h / 0 °C

With hydrogenchloride; sodium acetate; triethylamine; In ethanol;
DOI:10.1055/s-1989-27393