methyl (2S)-2-[[(4-methylphenyl)sulfonyl]amino]-4-(phenylseleno)butanoate

Base Information

Chemical Name:methyl (2S)-2-[[(4-methylphenyl)sulfonyl]amino]-4-(phenylseleno)butanoate
CAS No.:960004-39-1
Molecular Formula:C₁₈H₂₁NO₄SSe
Molecular Weight:426.395
Hs Code.:

Synonyms:methyl (2S)-2-[[(4-methylphenyl)sulfonyl]amino]-4-(phenylseleno)butanoate

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Chemical Property of methyl (2S)-2-[[(4-methylphenyl)sulfonyl]amino]-4-(phenylseleno)butanoate

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Technology Process of methyl (2S)-2-[[(4-methylphenyl)sulfonyl]amino]-4-(phenylseleno)butanoate

There total 5 articles about methyl (2S)-2-[[(4-methylphenyl)sulfonyl]amino]-4-(phenylseleno)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1190409-86-9
methyl (2S)-2-[[(4-methylphenyl)sulfonyl]amino]-4-iodo-butanoate

: 1666-13-3
diphenyl diselenide

: 960004-39-1
methyl (2S)-2-[[(4-methylphenyl)sulfonyl]amino]-4-(phenylseleno)butanoate

Guidance literature:: diphenyl diselenide; With sodium tetrahydroborate; In ethanol; at 8 - 21 ℃; Inert atmosphere;

methyl (2S)-2-[[(4-methylphenyl)sulfonyl]amino]-4-iodo-butanoate; In ethanol; at 20 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1021/ja9063475

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: C₁₇H₁₉NO₄SSe

: 960004-39-1
methyl (2S)-2-[[(4-methylphenyl)sulfonyl]amino]-4-(phenylseleno)butanoate

Guidance literature:: In diethyl ether; at 25 ℃; for 0.0833333h;
DOI:10.1039/b712861d

Reference yield:

: C₁₁H₁₄INO₄S

: 960004-39-1
methyl (2S)-2-[[(4-methylphenyl)sulfonyl]amino]-4-(phenylseleno)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / dichloromethane / 24 h / 20 °C / Inert atmosphere

2: sodium tetrahydroborate / ethanol / 8 - 21 °C / Inert atmosphere

With sodium tetrahydroborate; thionyl chloride; In ethanol; dichloromethane;
DOI:10.1021/jo101790z