4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylcyclohexanecarboxamide

Base Information

Chemical Name:4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylcyclohexanecarboxamide
CAS No.:1421932-35-5
Molecular Formula:C₂₄H₃₄N₄OS
Molecular Weight:426.626
Hs Code.:

Synonyms:4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylcyclohexanecarboxamide

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Chemical Property of 4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylcyclohexanecarboxamide

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Technology Process of 4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylcyclohexanecarboxamide

There total 8 articles about 4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylcyclohexanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421922-92-0
4-(bromoacetyl)-N-methylcyclohexanecarboxamide

: 1421922-06-6
2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylphenyl]ethanethioamide

: 1421932-35-5
4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylcyclohexanecarboxamide

Guidance literature:: In isopropyl alcohol; at 70 ℃; for 1h;

Reference yield:

: 619-81-8,619-82-9,1076-97-7
cyclohexane-1,4-dicarboxylic acid

: 1421932-35-5
4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylcyclohexanecarboxamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride / chloroform; N,N-dimethyl-formamide / 24 h / 20 °C / Cooling with ice

2.1: tetrahydrofuran / 3 h / Cooling with ice; Sealed tube

3.1: chloroform / 1.5 h / 20 °C / Cooling with ice

3.2: 0.83 h / 20 °C / Cooling with ice

4.1: isopropyl alcohol / 1 h / 70 °C

With oxalyl dichloride; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 16213-85-7
(2,5-dimethylphenyl)acetonitrile

: 1421932-35-5
4-{2-[4-({(E)-[ethyl(methyl)amino]methylidene}amino)-2,5-dimethylbenzyl]-1,3-thiazol-4-yl}-N-methylcyclohexanecarboxamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: nitric acid / 0.5 h / Cooling with ice

2.1: hydrogenchloride; O,O-Diethyl hydrogen phosphorodithioate / ethyl acetate / 24 h / 20 °C

3.1: ammonium chloride; iron; water / ethanol / 2 h / Reflux

4.1: oxalyl dichloride / chloroform / 0.17 h / 20 °C

4.2: 24 h / 20 °C

5.1: isopropyl alcohol / 1 h / 70 °C

With hydrogenchloride; oxalyl dichloride; water; nitric acid; iron; ammonium chloride; O,O-Diethyl hydrogen phosphorodithioate; In ethanol; chloroform; ethyl acetate; isopropyl alcohol;